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The paper describes a method for the quantitative comparison of slightly differing infrared spectra. The method is based on a comparison of the differences in absorbance of some selected band pairs which represent identification features of infrared spectra. An optimal combination of band pairs was chosen using two methods: a graphical method based on the validity of Beer's law (method I) and a purely statistical method (method II). The spectra characterized by the selected features were compared and the significance of differences between them was tested using the mathematical Hotelling's T2 test. It was found that the method developed enables the quantitative and objective evaluation of the statistical significance of differences between compared spectra. 相似文献
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Application of the micro-FTIR spectroscopy, Raman spectroscopy and XRF method examination of inks 总被引:4,自引:0,他引:4
In routine examination of inks on questioned documents non-destructive analytical methods, such as microscopic and optical techniques are applied first. However, they are often insufficient to identify the inks used for the preparation of the document. In such cases, it is necessary to apply chemical methods that normally cause partial destruction of the examined material. The aim of this work was to evaluate the possibility of discrimination between inks by the use of spectrometric methods, i.e. micro-FTIR spectroscopy, Raman spectroscopy and XRF. About 70 samples of blue and black ballpoint pen and gel inks were examined. It was found that about 90% of the samples of the same type and colour could be distinguished using these methods. 相似文献
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This paper introduces the Special Issue on the languages of performing arts and is therefore aimed at designing how the context of the latter can be illuminated by socio-semiotic and multimodal approaches to communication. In this Special Issue, performances and performing arts are described as multimodal semiotic acts that co-deploy a range of semiotic resources to produce and construct meanings across different cultures and ages. Seen as dynamic and interactive processes of meaning-making, their analysis calls for new and multidisciplinary frameworks which are collected in this Special Issue. The introduction gives an overview of these papers and discusses their range of diverse phenomena, both live and recorded, including theatre performances and films, art installations, opera, as well as reading out aloud. By outlining the significance and contribution of different disciplines and fields of studies to the broad area of performance studies, the chapter argues the case for innovative approaches that can extend theories and analyse aesthetic and performative practices in context. With the help of some case studies, it provides guidelines for the reading and interpretation of the several theoretical discussions and practical case studies presented to encourage further multidisciplinary research on these domains. 相似文献
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Janina Beiser‐McGrath 《Swiss Political Science Review》2019,25(3):203-225
Research on government repression often focuses on the comparison between states over time and provides little insight about the targets of repression within a state. This article unpacks government repression against different ethnic groups. It argues that non‐democratic governments use pre‐emptive and targeted repression against ethnic groups that are discriminated, strong, or have a history of protest or rebellion in order to prevent future ethnic rebellions. For democratic governments, on the other hand, the cost of pre‐emptive repression is too high. The article tests this argument in a quantitative analysis of government‐group dyads. It finds at least partial support for some implications of the argument: Autocratic governments use more repression than democracies against discriminated groups, but only when they are also weak, and against groups with a history of protest. There is little evidence that regimes of either type respond to previous violent mobilization or group strength with repression. 相似文献
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International legal scholars have identified and argued for and against new forms of non-consent-based international law. We study variation in Brazilian public opinion about adherence to international law created in three different ways: through a consent-based multilateral treaty, by the U.N. Security Council with the participation of Brazil, and by the U.N. Security Council without the participation of Brazil. Information that Brazil has participated in creating the international legal obligation through a multilateral treaty or membership on the Security Council yields levels of support for adherence to the legal obligation that are similar to those found when the origins of the legal obligation are generic. Information that the international legal obligation was created without Brazil’s participation, on the other hand, results in reduced support for compliance. This difference, which is particularly concentrated among highly educated respondents, is not driven by reduced concerns about reputational consequences or sanctions. Our results suggest that the increased use of non-consent-based forms of international law might be challenged by a lack of public support for compliance. 相似文献
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Janina Zięba‐Palus Ph.D. Aleksandra Michalska M.Sc. 《Journal of forensic sciences》2014,59(4):943-949
Micro‐Raman spectroscopy was applied to forensic identification of pigments in paint chips and provided differentiation between paint samples. Sixty‐six blue automotive paint samples, 26 solid and 40 metallic were examined. It was found that the majority of the collected Raman spectra provided information about the pigments present. However, in some cases, fluorescence precluded pigment identification. Using laser excitation at longer wavelengths or pretreatment to effect photobleaching often resulted in reduced fluorescence, particularly for solid color samples, and allowed pigment identification. The examined samples were compared pairwise taking into account number, location, and intensity of absorption bands in their infrared spectra. The estimated discrimination power ranged from 97% for solid paint samples to 99% for metallic paint samples. 相似文献
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Neutze J Grundmann D Scherner G Beier KM 《International journal of law and psychiatry》2012,35(3):168-175
Current knowledge about risk factors for child sexual abuse and child pornography offenses is based on samples of convicted offenders, i.e., detected offenders. Only few studies focus on offenders not detected by the criminal justice system. In this study, a sample of 345 self-referred pedophiles and hebephiles was recruited from the community. All participants met DSM-IV-TR criteria for pedophilia or hebephilia (paraphilia not otherwise specified), were assured of confidentiality, and self-reported lifetime sexual offending against prepubescent and/or pubescent children. Two sets of group comparisons were conducted on self-report data of risk factors for sexual reoffending. Measures of risk factors address the following dimensions identified in samples of convicted offenders: sexual preferences (i.e. co-occurring paraphilias), sexual self-regulation problems, offense-supportive cognitions, diverse socio-affective deficits, and indicators of social functioning (e.g., education, employment). Men who admitted current or previous investigation or conviction by legal authorities (detected offenders) were compared with those who denied any detection for their sexual offenses against children (undetected offenders). Group comparisons (detected vs. undetected) were further conducted for each offense type separately (child pornography only offenders, child sexual abuse only offenders, mixed offenders). Although there were more similarities between undetected and detected offenders, selected measures of sexual-self regulation problems, socio-affective deficits, and social functioning data demonstrated group differences. 相似文献
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