大孔吸附树脂纯化番石榴叶总皂苷的工艺研究 |
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作者姓名: | 鄢文 程冰洁 刘强 黄海军 任沁沁 陈宝田 周迎春 |
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作者单位: | 南方医科大学南方医院中医内科 广东广州510515 |
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基金项目: | 国家自然科学基金,广东省自然科学基金 |
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摘 要: | 目的:研究SA 1型大孔吸附树脂吸附提取番石榴叶总皂苷的工艺条件及参数.方法:以番石榴叶总皂苷为考察指标,研究树脂吸附容量、洗脱溶媒及其用量等工艺条件.结果:通过SA 1型大孔树脂吸附后,先经3倍BV(床体积)水洗,再以800 ml/L乙醇为洗脱溶媒.4倍BV洗脱效果最佳,总皂苷纯度可达55.3%.结论:此法能较好地分离纯化番石榴叶总皂苷,是简便、可行的提取方法.
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关 键 词: | 大孔吸附树脂 番石榴叶总皂苷 提取工艺 |
收稿时间: | 2007/11/16 0:00:00 |
Purification Process of Total Saponin ofPsidium Guajava L. with SA-1 Macroreticular Resin |
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Authors: | YAN Wen CHENG Bing-jie LIU Qiang HUANG Hai-jun REN Qin-qin CHEN Bao-tian ZHOU Ying-chun |
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Abstract: | Objective:To study the technological parameters of purification of Psidium Guajava L. with SA-1 macroreticular resin.Methods:The absorptive capacity,elution dissolvant and its volume were studied through a lot of experiments using the content of total saponins of Psidium Guajava L. as index. Results: It was firstly washed with 3 times of bed volume (BV) of distilled water,then eluted with 4 BV of 800 ml/L ethanol after macroreticular resin absorbing. The effect of elution with 4 BV of dissolvent was the most, and the purity of total saponins of Psidium Guajava L. was up to 55.3%.Conclusion:This method is feasible and simple, and it can be used for absorbing and purifying the total saponins of Psidium Guajava L.. |
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Keywords: | Macroreticular resin Total saponins of Psidium Guajava L Extraction technique |
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