| 气/质联用法检测鱼藤中鱼藤酮 |
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| 引用本文： | 韩凤鸣,李晓东,赖仕均,卢政煜.气/质联用法检测鱼藤中鱼藤酮[J].刑事技术,2011(3):35-36. |
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| 作者姓名： | 韩凤鸣 李晓东 赖仕均 卢政煜 |
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| 作者单位： | 广东省深圳市公安局刑事科学技术研究所,518000 |
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| 摘 要： | 目的建立气相色谱/质谱联用法检测鱼藤中鱼藤酮的方法。方法将鱼藤根净化处理后使用三氯甲烷浸提,提取液浓缩后经FINNIGAN POLARIS Q型GC/MS气质联用仪检测。结果通过质谱库匹配检出鱼藤酮。结论本方法操作简便、结果准确,易于推广应用,适用于鱼藤酮的检测。
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| 关 键 词： | 鱼藤酮 鱼藤 气相色谱/质谱联用 |
Determination of rotenone in derris by GC/MS |
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| HAN Feng-ming,LI Xiao-dong,LAI Shi-jun,et al.Determination of rotenone in derris by GC/MS[J].Forensic Science and Technology,2011(3):35-36. |
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| Authors: | HAN Feng-ming LI Xiao-dong LAI Shi-jun |
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| Institution: | HAN Feng-ming,LI Xiao-dong,LAI Shi-jun,et al(Institute of Forensic Sciences,Bureau of Public Security of Shenzheu City,Shenzhen 518000,China) |
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| Abstract: | Objective To establish a GC/MS method for detecting rotenone in derris.Method Rotenone was extracted by chloroform in roots of derris and analyzed by GC/MS.Result The mass spectrum of sample was matched with rotenone in NIST MS library.Conclusion The method is simple,accurate,easy to use,and suitable for routine analysis. |
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| Keywords: | rotenone derris gas chromatography/mass spectrum |
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