| 生物检材中微量斑蝥素的检验 |
| |
| 引用本文： | 吴维蓉,孟品佳,李宜春.生物检材中微量斑蝥素的检验[J].中国法医学杂志,1992(3). |
| |
| 作者姓名： | 吴维蓉 孟品佳 李宜春 |
| |
| 作者单位： | 中国刑警学院，中国刑警学院，中国刑警学院 沈阳 110035，沈阳 110035，沈阳 110035 |
| |
| 摘 要： | 本文提出了用酸解法分离提取生物检材中的斑蝥素,并提供了一种新的薄层显色方法。以烯丙异丙巴比妥为内标的气相色谱法测定斑蝥素含量,准确可靠。回收率可达85％。应用该法测定了中毒动物死后的体内分布。
|
| 关 键 词： | 斑蝥素 酸解提取法 气相色谱法 薄层色谱法 死后体内分布 |
DETECTION OF MICRO CANTHARIDIN BIOLOGICOL MATERIALS |
| |
| Wu Weirong Meng Pinjia Li Yichun Criminal Police Institute of China,Shenyang.DETECTION OF MICRO CANTHARIDIN BIOLOGICOL MATERIALS[J].Chinese Journal of Forensic Medicine,1992(3). |
| |
| Authors: | Wu Weirong Meng Pinjia Li Yichun Criminal Police Institute of China Shenyang |
| |
| Institution: | Wu Weirong Meng Pinjia Li Yichun Criminal Police Institute of China,Shenyang 110035 |
| |
| Abstract: | A simple isolation of cantharidin from biological materials by acid hydrolysis and a new colord developemental method of TLC were established.Results of quantitative measurement of cantharidin by GC using aprobarhital as an internal standard were reliable. The mean recoveries from spiked specimens were 85%.These procedures were applied to study the postmortem distribution of cantharidin in poisoned animals. |
| |
| Keywords: | Cantharidin Acid hydrolysis GC TLC Postmortem distribution |
| 本文献已被 CNKI 等数据库收录！ |
