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| 固体进样杆-GC/MS-SIM技术检验头发中6-单乙酰吗啡 | |
| 引用本文： | 李舒平,谢体慧,赖富平,吴承华,钟春明,袁晓宇,曾东,李明. 固体进样杆-GC/MS-SIM技术检验头发中6-单乙酰吗啡[J]. 刑事技术, 2011, 0(6): 27-29 |
| 作者姓名： | 李舒平 谢体慧 赖富平 吴承华 钟春明 袁晓宇 曾东 李明 |
| 作者单位： | 1. 福建龙岩市公安局刑事科学技术所,364000 2. 福建龙岩市新罗分局刑事科学技术室,364000 |
| 摘 要： | 目的建立固体进样杆-GC/MS-SIM技术,检测人头发中毒品海洛因的主要代谢产物6-单乙酰吗啡的方法。方法样品头发洗净剪碎后,经MSTFA衍生化,采用GC/MS-SIM定性定量分析。结果 6-单乙酰吗啡在浓度0.1ng/mg～18.0ng/mg范围内线性相关系数为0.9972,方法检出限为0.1ng/mg。结论本方法头发使用量小,准确度、精密度良好、灵敏度高,是高效、快速、实用的测定头发中6-单乙酰吗啡的方法。 |
| 关 键 词： | 固体进样杆 气-质联用法 毛发分析 6-单乙酰吗啡 |
Determination of O6-monoacetylmorphine in hair by GC/MS |
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| LI Shu-ping,XIE Ti-hui,LAI Fu-ping,et al. Determination of O6-monoacetylmorphine in hair by GC/MS[J]. Forensic Science and Technology, 2011, 0(6): 27-29 | |
| Authors: | LI Shu-ping XIE Ti-hui LAI Fu-ping et al |
| Affiliation: | LI Shu-ping,XIE Ti-hui,LAI Fu-ping,et al(Public Security Bureau of Longyan,Fujian Province,364000,China) |
| Abstract: | A method for determination of O6-monoacetylmorphine in hair by gas chromatography-mass spectrometry(GC-MS) with subsection SIM mode was developed.The hair sample was derivatived with MSTFA and then analyzed qualitatively and quantitatively.The results show that linear range was 0.1ng/mg~18.0ng/mg with a correlation coefficient of 0.9972 and the detection limit for nitrate nitrogen was 0.1 ng/mg.The method is simple,sensitive and can meet the test request of O6-monoacetylmorphine in hair. |
| Keywords: | chromatoprobe GC/MS-SIM hair analysis O6-monoacetylmorphine |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |