| 生物材料中溴氰菊酯的内标监控高效液相色谱分析方法研究 |
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| 引用本文： | 黄启文,廖林川,郭平,李章万,江焘.生物材料中溴氰菊酯的内标监控高效液相色谱分析方法研究[J].中国法医学杂志,1993(3). |
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| 作者姓名： | 黄启文 廖林川 郭平 李章万 江焘 |
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| 作者单位： | 成都市医药采购供应站，华西医科大学，华西医科大学，华西医科大学，华西医科大学 成都 610041，成都 610041，成都 610041，成都 610041 |
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| 摘 要： | 本文经实验研究建立了以反式二氯苯醚酯为监控内标反相高效液相色谱检测生物材料中溴氰菊酯的方法。通过空白兔肝添加试验验证了方法的回收率,工作曲线线性及数份样品的重视性。结果满意。并通过染毒动物试验验证了方法的实用性。
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| 关 键 词： | 反相高效液相色谱法 溴氰菊酯 |
DETERMINATION OF DELTAMETHRIN IN BIOLOGICIAL MATRIALS BY RPHPLC USING INTERNAL STANDARD MONTORING |
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| Huang Qiweng Liao Linchuan Guo Ping Li Zhangwan Jiang Tao West China University of Medical Sciences Chengdu.DETERMINATION OF DELTAMETHRIN IN BIOLOGICIAL MATRIALS BY RPHPLC USING INTERNAL STANDARD MONTORING[J].Chinese Journal of Forensic Medicine,1993(3). |
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| Authors: | Huang Qiweng Liao Linchuan Guo Ping Li Zhangwan Jiang Tao West China University of Medical Sciences Chengdu |
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| Abstract: | In this paper, anexperimental study on the selection and companionship of internal standard, extraction and cleanning up method, and eomposition of themobile phase for determinating the deltamethrin in biological materials was performed. After that, a RPHPLC method was established under the control of the internal stantard transpermethrin. The recovery rates from the spiked rabbit's liver (at the levis of 0.2-20mg/kg.) were around 90% The eoffecient of variation of determination for 8 times was 2. 31%. The results showed that this method has a satisfactory reproducibility and can be used for determinating deltamethrin in tissues, organs and body fluids from poisoned animals. |
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| Keywords: | RPHPLC Deltamethrin |
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