Quantified Explosives Transfer on Surfaces for the Evaluation of Trace Detection Equipment |
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Authors: | Maggie Tam PhD Pierre Pilon PhD Hafid Zaknoun MSc |
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Institution: | Science and Engineering Directorate, Canada Border Services Agency, , Ottawa, K2E 6T7 Ontario, Canada |
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Abstract: | Trace explosive test surfaces are often required for the evaluation of trace detection equipment to determine the equipment performance. Test surfaces of C‐4, Detasheet, Semtex‐H, TNT, and HMTD were prepared by transferring trace amount of explosive deposited on polytetrafluoroethylene (PTFE) transfer strips onto different surfaces (Kraft paper, hard plastic, woven fabric, and soft vinyl). The amount of explosive transferred was deduced from the amount of explosive remaining on the PTFE strips after transfer, as quantified by direct analysis using tandem mass spectrometry with thermal desorption. From the data set of over 2000 transfers, we experienced lower transfer efficiency for Semtex‐H and Detasheet, and for soft vinyl and hard plastic. However, the rapid quantification mass spectrometric method allowed the transfer efficiency to be determined for all test surfaces used in an evaluation of trace explosive detectors, thereby permitting only the test surfaces with desired transfer to be accepted for the assessment. |
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Keywords: | forensic science explosive detection mass spectrometry 2 4 6‐trinitrotoluene C‐4 Semtex‐H Detasheet
HMTD
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