| 鸦片中主要成分的检验 |
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| 引用本文： | 吴展频.鸦片中主要成分的检验[J].中国法医学杂志,1993(3). |
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| 作者姓名： | 吴展频 |
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| 作者单位： | 福建省刑事科学技术研究所 福州 |
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| 摘 要： | 本文采用Seppak C_(18)小柱固相萃取鸦片中的五种主要成分,以反相高效液相色谱法,甲醇—甲酸—三乙胺水(35:1.5:0.5:63)为流动相,检验五种成分,各成分均有良好的回收率。方法简单、快速、准确。
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| 关 键 词： | 鸦片 高效液相色谱 固相萃取 |
DETERMINATION OF MAJOR ALKALOIDS IN OPIUM BY SOLID- PHASE EXTRACTION AND REVERSED-PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY |
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| Wu Zhanpin Fujian Forensic Science Institute Fuzhou.DETERMINATION OF MAJOR ALKALOIDS IN OPIUM BY SOLID- PHASE EXTRACTION AND REVERSED-PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY[J].Chinese Journal of Forensic Medicine,1993(3). |
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| Authors: | Wu Zhanpin Fujian Forensic Science Institute Fuzhou |
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| Abstract: | A simple and rapid method for the isolation and detection of five major alkaloids in opium by Sep --pak C_(18) cartridges sol(d--phase extraction and high--performance liquid chromatography is reported. The recoveries by using of the eartridage were excellent for most alkaloids. Separation of each alkaloid peak from each other on the high--performance liquid chromatography was satisfactory by using of μ--Bondapak C_(18) column and methanol--methanoic acid--triethylamine--water (35: 1.5: 0.5: 63,v/v) as mobile phase. |
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| Keywords: | Opium HPLC Solid—phase extraction |
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