| 应用SPME-GL／MS检测放火现场中助燃剂的研究 |
| |
| 引用本文： | 张成功,王长富,凌友青,邵致远,丁敏菊.应用SPME-GL／MS检测放火现场中助燃剂的研究[J].中国司法鉴定,2004(1):18-20. |
| |
| 作者姓名： | 张成功 王长富 凌友青 邵致远 丁敏菊 |
| |
| 作者单位： | 上海市刑事科学技术研究所,上海,200083 |
| |
| 摘 要： | 运用GC/MS拜利用自制的萃取、加热装置,研究在纵火现场助燃剂一汽油、煤油、柴油检测中固相微萃取的萃取温度和萃取时间对检测灵敏度的影响,确定了适于实际检案中采用的萃取时间和萃取温度.此法测定汽油、煤油、柴油的检出限分别为0.65 pl/ml、1.63pl/ml和1.63 pl/ml.
|
| 关 键 词： | SPME GC/MS 汽油 煤由 柴油 |
| 文章编号： | 1671-2072(2004)01-0018-03 |
| 修稿时间： | 2003年9月17日 |
Determination of Combustion Improvers in Fire Debris |
| |
| ZHANG Cheng-gong,WANG Chang-fu,LING You-qing,et al..Determination of Combustion Improvers in Fire Debris[J].Chinese Journal of Forensic Sciences,2004(1):18-20. |
| |
| Authors: | ZHANG Cheng-gong WANG Chang-fu LING You-qing |
| |
| Abstract: | A simple method for the determination of Combustionimprovers, such as gasoline, kerosene and diesel oil, has been developedby GC/MS, along with extracting and heating devices designed by theauthor. It was found that extracting temperature and moment in SPMEinfluenced the sensitivity of the analysis. In the study, the optimal analyzingconditions were established, and under the condition, the detection limitsfor gasoline, kerosene and diesel oil were 0.65pl/ml, 1.63pl/ml and 1.63pl/ml respectively. |
| |
| Keywords: | gasoline kerosene diesel oil SPME GC/MS |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
