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| 人体血液中吗啡的定性定量分析 | |
| 引用本文： | 裴茂清,丛培峰,狄碧.人体血液中吗啡的定性定量分析[J].刑事技术,2004(6):6-7. |
| 作者姓名： | 裴茂清 丛培峰 狄碧 |
| 作者单位： | 1. 广东省公安厅刑事技术中心,广州,510050 2. 广东省江门市公安局刑警支队,529000 3. 广州铁路公安处,广州,510140 |
| 摘 要： | 目的 建立人体血液中吗啡的定性定量分析方法。方法 经过丙酸酐衍生化法 ,利用气质联用和气相色谱氮磷检测器对吗啡丙酸酐衍生物进行定性定量分析。结果 确定了人体血液中吗啡的气质联用和气相色谱氮磷检测器定性定量分析的色谱条件、吗啡气相色谱氮磷检测器定量分析的线性范围及吗啡最小检出量0 1ng。结论 该方法定性定量结果准确、可靠 ,定量线性范围可满足实际办案需要 ,为吸食鸦片类毒品人群血液中吗啡的定性定量分析提供了分析方法和依据 |
| 关 键 词： | 吗啡 衍生化 定性定量 |
| 文章编号： | 1008-3650(2004)06-0006-02 |
| 修稿时间： | 2003年5月9日 |
Qualitative and quantitative analysis of morphine in hunman blood |
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| PEI Mao-qing,CONG Pei-feng,DI Bi..Qualitative and quantitative analysis of morphine in hunman blood[J].Forensic Science and Technology,2004(6):6-7. | |
| Authors: | PEI Mao-qing CONG Pei-feng DI Bi |
| Abstract: | Objective TO establish a method for qualitative and quantitative analysis of morphine in human blood. Method After acid anhydride derivating, morphine and acid anhydride derivation were analyzed qualitatively and quantitatively by GC/MS and GC/NPD. Result The conditions and linearity range of qualitative and quantitative analysis of morphine in human blood by GC/MS and GC/NPD was determined. Conclusion The method is accurate and reliable, the linearity range meets the need of the determination of morphine in blood. |
| Keywords: | morphine derivate qualitative and quantitative analysis |
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