| GC/NPD、GC/FID分析生物样品中的氟乙酰胺 |
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| 作者姓名： | Feng SZ Yu ZS |
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| 作者单位： | 公安部物证鉴定中心 |
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| 摘 要： | 报道了用ＧＣ／ＮＰＤ、ＧＣ／ＦＩＤ分析生物试样中的氟乙酰胺的方法。在１ｇ肝组织中加入５．０μｇ氟乙酰胺,回收率为８５．１％,ＲＳＤ为５．３９（ｎ＝７）;１ｍｌ血中加５μｇ,回收率为８５．１％,ＲＳＤ为７．１１％;在１ｇ胃组织中加入１０μｇ,回收率为８１．６％,ＲＳＤ为１０．１％（ｎ＝７）。研究的方法经动物实验和中毒案件的应用,效果较好
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| 关 键 词： | 氟乙酰胺 生物脏器 GC／NPD GC／FID |
Analysis of fluoroacetamide in biological samples with GC/NPD,GC/FID |
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| Feng SZ,Yu ZS.Analysis of fluoroacetamide in biological samples with GC/NPD,GC/FID[J].Journal of Forensic Medicine,1999,15(2):91-2, 125. |
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| Authors: | Feng S Z Yu Z S |
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| Institution: | Institute of Forensic Sciences, Ministry of Public Security, Beijing 100038, P. R. China. |
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| Abstract: | A GC/NPD and GC/FID method has been developed for the analysis of fluoroacetamide
(1081),using AC-20 and FFAP capillary column.The recovery is 85.1%(RSD 5.4%), 85.1%(RSD 7.1%)
and 81.6%(RSD 10.1%) in liver,whole blood and stomach tissue,respectively. |
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| Keywords: | fluoroacetamide liver whole blood GC/NPD GC/FID |
| 本文献已被 CNKI PubMed 等数据库收录！ |
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