J. Brunnée; S.J. Toope,Legitimacy and Legality in International Law: An Interactional Account,Cambridge University Press,Cambridge 2010, xviii + 411 pp., UK£60/US$105, ISBN 978-0-521-88065-7 (hardback); UK£29.99/ US$55, ISBN 978-0-521-70683-4 (paperback). doi: 10.1017/S0165070X11200056

Netherlands International Law Review -     

M. Boersma,Corruption: A Violation of Human Rights and a Crime under International Law?, Intersentia,Antwerp 2012, xxiii + 490 pp. ISBN 978-1-78068-105-4.

Netherlands International Law Review -     

A.G. Oude Elferink,The Delimitation of the Continental Shelf between Denmark,Germany and the Netherlands: Arguing Law,Practicing Politics?, Cambridge University Press,Cambridge 2013, xxv + 508 pp. ISBN 978-1-107-04146-2 (hardback).

Netherlands International Law Review -     

N,N-二烯丙基-5-甲氧基色胺片剂的GC/MS检验

目的 建立N,N-二烯丙基-5-甲氧基色胺的气相色谱-质谱(GC/MS)定性分析方法。方法 未知片剂样品用甲醇超声溶解,吸取上清液采用气相色谱-质谱(GC/MS)联用仪检测。结果 测得未知组分(tR=10.45min)的质谱特征碎片峰(m/z)信息为110.1(基峰)、270.1、174.1、160.1、145.0、130.1和117.1。查阅资料并对该组分的质谱图谱进行解析,鉴定为N,N-二烯丙基-5-甲氧基色胺,属于色胺类化合物。结论 该方法简单,准确,可用于N,N-二烯丙基-5-甲氧基色胺的鉴定。