纸张经茚三酮显现指印后的变色现象

目的研究经茚三酮显现指印后纸质检材的变色规律、产生条件及解决方法。方法比较不同茚三酮显现条件，显现后不同保存条件下各种纸质检材的变色现象。结果经茚三酮显现指印后纸质检材的保存环境中，当温度、湿度达到一定条件时，大部分纸质检材会发生不同程度的变色现象。结论经茚三酮显现后的纸质检材要采取适当的方法保存。影响纸张变色的决定性因素为检材所保存的温度和湿度。环境温度在25℃以上并且湿度在60％以上，经茚三酮药液显现的白色纸张保存24h后都会有变色的可能，48h后绝大部分白色纸张会发生变色。     

LED多波段光源显现人民币上潜指印的研究

目的研究显现、提取遗留在人民币上潜在指印的方法。方法采用荧光试剂罗丹明6G对人民币进行染色处理,以LED多波段光源输出的波长为520nm的绿光照射检材,透过580nm的带通型干涉滤光镜观察指印的显现效果,并拍照提取。结果获得亮纹线暗背景的指印图像,指印纹线清晰,反差良好,特征丰富,具备良好的检验鉴定条件。结论 LED多波段光源输出的波长为520nm的绿光与罗丹明6G染色指印的吸收特性吻合,是显现、提取遗留在人民币上潜在指印的良好光源。     

短波紫外反射照相显现铝制板汗液指印效果差异分析

目的 分析短波紫外反射照相显现铝制板框上汗液指印效果差异形成的原因.方法 利用短波紫外反射照相并用不同的打光方式对铝制板框汗液指印进行显现.结果 打光的角度不同,汗液指印的显现效果截然不同,并且在小角度入射的情况下,铝制板框上的汗液指印显现效果和玻璃载玻片上的汗液指印显现效果也明显不同,铝对短波紫外高反射率的特性引起了汗液指印显现效果的不同.结论 针对铝制板类的检材,在利用短波紫外进行汗液指印显现时需要明确不同情况下相应的显现效果.     

紫外激光技术显现潜在指印的研究

目的研究显现潜在指印的新技术。方法用自主研发的266nm短波紫外线输出的ND：YAG激光器作为激发光源激发渗透性客体表面的潜在指印,使指印发出荧光。结果能有效显现出亮纹线暗背景的潜在指印发光图像。结论利用该紫外激光技术可以显现纸张等渗透性客体表面的潜在指印。     

远红外加热无损显现渗透性客体上指印初探

在指印显现实践中,渗透性客体上的汗液指印显现方法主要是有损显现,对此,本实验尝试建立远红外加热无损显现渗透性客体上汗液指印,介绍如下。1材料和方法1.1材料检材加温设备：HGXJ-807潜在手印无损显现系统（上海恒光警用器材有限公司）,HGXJ-447nm激光生物显现仪（上海恒光警用器材有限公司）,NIKON单反数码照相机,447nm干涉滤光镜。1.2方法（1）将HGXJ-807潜在手印无损显现系统通上电,预加热5min~6min,箱内温度设置185℃。     

DFO指印显现技术及应用

本文介绍了DFO指印显现技术配方、操作方法和系统应用实验研究结果,发现DFO方法可以有效显现各种纸张上的汗液指印和血指印,对陈旧指印和微弱指印显现效果良好,显现成功率远远高于茚三酮和茚三酮/氯化锌方法,在实际办案中也取得了理想的显现效果。     

遗留不同时间的潜在汗液指印紫外发光显现技术的实验研究

目前对于渗透性客体上的潜在汗液指印,紫外发光显现技术是一种行之有效且无损的方法。但是对同一枚指印,可能因为其遗留的时间不同,紫外发光显现有不同的显现效果,遗留时间较短,显现的效果可能好点,遗留时间较长,显现效果可能较差或者不能显现。本实验以笔记本纸上的潜在汗液指印(皮脂型潜在汗液指印)为样本,采用紫外发光显现技术测试能够显现潜在汗液指印遗留的最长时间。本实验中,笔记本纸上的潜在汗液指印分别放置1、7、40天,然后采用紫外发光显现技术显现指印,得到不同的显图1紫外发光显现技术装置示意图2实验步骤(1)将拍摄所需器材准备…     

浅议DFO石油醚配方显现指印存在的问题及解决办法

近年来,一种新型的荧光试剂——1,8-Diazafluoren-9-onc(DFO)被广泛地应用于显现各类纸张上的汗液指印。它是与汗液指印中的氨基酸反应生成一种具有强烈荧光的淡紫色产物。这种方法比目前使用的茚三酮法显现率高,效果好。 我们利用公安部物证鉴定中心研制推广的DFO指印显现技术在实际工作中得到了较好的效果,但也发现了一些问题,下面就存在的问题及解决办法与同行们进行探讨:     

DFJ-1型定向反射镜及应用

本文介绍了用于拍照显现潜在指印的DFJ-1型定向反射镜,该镜结构简单,使用方便,能够产生理想的定向反射效果,可以有效显现光滑平面表面上的潜在指印和加强微弱指印。     

紫外光谱成像技术显现潜在油汗混合指印的初步探索

目的研究运用紫外光谱成像技术显现潜在油汗混合指印的可行性和方法。方法使用紫外光谱成像仪获取典型潜在油汗混合指印的光谱影像数据资料,比较不同数据处理软件的分析结果。结果紫外光谱成像技术具有显现潜在油汗指印的能力。结论紫外光谱成像技术能够成功显现非渗透性客体表面潜在油汗混合指印。     

Luminescent visualization of latent fingerprints by direct reaction with a lanthanide shift reagent.

The utilization of the lanthanide shift reagent tris (6,6,7,7,8,8,8-heptafluoro-2,2-dimethyl-3,5-octanedionato) europium (III) [Eu(fod)3] as a simple one-step reagent for the luminescent visualization of latent fingerprints has been investigated. UV excitation of Eu(fod)3-treated prints, achieved by using a hand-held UV lamp or a Polilight, results in an orange emission at 614 nm. Time-resolved imaging is not required for visualization. Visualization of latent fingerprints on paper under the conditions used, although good, was found to be inferior to that obtained by standard DFO (1,8-diazafluoren-9-one) treatment, whereas visualization of prints obtained on aluminum drink cans and galvanized iron proved superior to that obtained by Superglue/panacryl treatment. Eu(fod)3 treatment can also be used first without compromising subsequent ninhydrin or DFO treatment, making it a 'nothing-to-lose" reagent.     

Determination of efficacy of fingermark enhancement reagents; the use of propyl chloroformate for the derivatization of fingerprint amino acids extracted from paper

The analysis of the constituents of fingerprints has been described numerous times, mainly with the purpose of determining the aging effect on fingerprints or showing the differences between donors or groups of donors. In this paper we describe the use of derivatized amino acids to determine the efficacy of the visualization reagents 1,8-diazafluoren-9-one (DFO) and ninhydrin. At present certain conditions are used for the application of these reagents, as determined by trial-and-error investigations, to the effect on fingerprints. The recovery of amino acids from a porous surface can be used as a measure for the efficacy of a visualization agent.In this paper we describe a method for the determination of the amount of amino acid left after reaction with well known fingerprint visualization reagents. This will allow a more scientific approach to method development for fingermark enhancement techniques. Furthermore, investigations on the influence of the concentration of fingermark amino acids, the order of application of and exposure time to reagents and the influence of age of the amino acids were carried out. These studies have resulted in a broader understanding of the mechanism involved in visualization of fingermarks using DFO and ninhydrin.     

TFD-2纸张手印快速显现系统的应用

目的介绍一种利用特殊的红外热成像技术显现常见纸张上汗潜手印的新方法。方法利用英国Foster4-Freeman公司生产的TFD-2纸张手印快速显现系统,通过特殊的红外热成像技术,使汗潜手印呈现强烈荧光,从而显现手印。结果红外热成像方法处理后,汗潜手印在特种激发光（带宽为450nm-510nm）激发下显出较强的橙色荧光;持续处理后,汗潜手印在自然光下呈棕褐色,并在短波紫外光源（254nm）激发下也可显出清晰连贯的手印纹线;而且,新鲜和陈旧手印均有较好的显现效果。结论TFD-2纸张手印快速显现系统显现纸张上汗潜手印的方法,具有操作简单、快速安全、无需化学试剂、显现效果明显的特点,适合推广使用。     

Visualization of Latent Fingerprint Corrosion on a Discharged Brass Shell Casing

Abstract:  Latent fingerprint visualization on discharged shell casings can provide good forensic evidence, particularly if the casing is recovered at the scene of a crime where a firearm has been discharged. Unfortunately, visualization of such latent fingerprints when they were deposited prior to discharge of the firearm is problematic as both increased temperature and abrasive friction can inhibit fingerprint visualization with conventional techniques. We present a case study that demonstrates latent fingerprint visualization on a discharged shell casing recovered 14 years ago from the scene of a homicide. Previous cyanoacrylate fuming of the casing had failed to reveal any fingerprints. We use a visualization technique in which a conducting carbon powder adheres preferentially to latent fingerprint corrosion of the casing surface, following the application of a potential of 2.5 kV to the casing. This technique presents opportunities for the review of old cases and for consideration of its use in current cases.     

碘热升华喷枪显现潜手印的应用研究

本文提出一种以石英灯为加热器的碘热升华喷枪显现潜手印的新方法。实验表明,该技术方法操作简便,适用范围广,手印显出率高,尤其是显现遗留在墙面、本色铝合金表面、UPVC表面的潜手印效果明显。     

“502”胶液体显现潜手印技术的研究

目的研究探索"502"胶溶液显现手印的方法.方法以石油醚为分散剂,添加对苯二酚作为显现增强剂,配制"502"胶显现液.结果能够显现非渗透客体上油质加、减层手印、加减层混合手印及普通汗潜手印,其显现效果与"502"胶熏显法非常相似.结论该方法具有方便、快捷、灵敏等特点,是"502"胶显现手印技术的重要补充.     

Enhancement of ninhydrin- or DFO-treated latent fingerprints on thermal paper

A new method for enhancement of ninhydrin or 1,8-diazafluoren-9-one (DFO)-treated latent fingerprints on thermal paper will be described. Most thermosensitive surfaces of thermal paper become dark when treated with DFO or ninhydrin petroleum ether (NPB) solution. This effect minimizes contrast between the developed fingerprints and the background. The new method described reduces this dark staining without removing the thermosensitive layer and parts of the developed fingerprints, as occurs with acetone washing. Through the new method, the developed fingerprints appear in sharp lines and high contrast. Extensive tests were performed, leading to an optimized working solution, which charges the paper with a minimum of chemicals, is cheap, and enables a large quantity of papers to be treated in a short time. The working solution contains commercially available, nonvolatile, nitrogenous organic compounds and can be used like the application of NPB solution by dipping.     

The Use of Liquid Latex to Recover Latent Fingerprints that are Covered in Debris from Exterior Glass Surfaces of Vehicles

The purpose of this research is to determine if latent fingerprints deposited on the exterior glass surfaces of vehicles, then covered in debris, can be recovered. Past research used liquid latex to lift soot to recover trace evidence. Recently, liquid latex has been used to recover latent fingerprints along the bottom of vehicles. In this study, a total of 216 latent fingerprints were deposited on the exterior windows of three vehicles. Three control and three experimental latent fingerprints were placed on each side window. The vehicles collected debris for either 2, 3, or 4 weeks. After debris collection, liquid latex was applied to the experimental sections. The underlying fingerprints were developed with white granular powder. Control fingerprints were developed directly with white granular powder. A chi-square test revealed a significant difference in fingerprint recovery between the control and liquid latex method (X² = 9.026, d.f. = 1, p = 0.003). An odds ratio determined that the control method increases the probability of latent fingerprint recovery by 2.68. Fisher's exact test indicated that there is no statistically significant difference between the detail of the recovered control and experimental fingerprints (p = 0.065). This study demonstrates that recovery of fingerprints is possible using the liquid latex method; however, the control method recovers more fingerprints on the glass exterior of vehicles. If latent fingerprints are thought to be present on the exterior glass surfaces of vehicles, the control method should be used to improve vehicle processing by investigators.     

Development of latent fingerprints on compact disc and its effect on subsequent data recovery

Chance fingerprints may be found on every type of surfaces of contact and when they are latent, need to be developed by various methods. The type of surface on which latent prints are to be developed is one of the important factors when a choice for a method of development is to be made. The matter becomes more crucial when the surface is unique like a compact disc containing digital data. In this case, to develop the fingerprints is not the only matter to be taken care of but also, is very important to select such a method which may not effect the stored data and its retrieval. In present investigation, various methods have been tried to develop fingerprints on the writing surface of a CD and results are discussed with respect to their development as well as its effect on stored data and data retrieval.     

指甲花醌显现纸张上汗潜手印初步研究

目的介绍一种用天然植物提取成分指甲花醌显现渗透性纸张表面汗潜手印的方法。方法利用指甲花醌能够和手印遗留物质中的氨基酸发生显色反应来显现手印。结果显现出的手印纹线在自然光下观察呈紫褐色,并且在540nm激发光源条件下,通过红色护目镜观察还有很强的荧光特征。结论指甲花醌显现法具有安全性高、健康环保、操作简单、显现效果明显的特点。