藻酸盐材料在提取深色织物上潜血足迹的应用

目的建立一种用藻酸盐齿科材料转印显现纺织物上血足迹的方法。方法依据藻酸盐能和纺织物上血足迹中的血结合,从而使足迹被转印到藻酸盐模上,并通过染色增强反差。结果藻酸盐印模材料转印法能够在不破坏织物客体的情况下清楚的反映出血足迹细节特征。结论藻酸盐类齿科材料能够转印、提取显现织物上血足迹,尤其是潜在血足迹,并反映出其细节特征。     

Lifting techniques for finger marks on human skin previous enhancement by Swedish Black powder — A preliminary study

An examination was done to investigate whether certain lifting techniques can lift recovered latent fingerprints on human skin surfaces of living subjects. For recovery Swedish Soot powder mixture (Swedish Black) was used.Donors intentionally placed fingerprints on the skin surface of living subjects. Finger marks were then in all cases recovered with Swedish Black powder. The procedure was repeated after 1 h and 4 h. Treated finger marks were secured and preserved as latent fingerprint evidence by different lifting processes. Having examined skin surfaces and finger marks we observed that the lifters such as white instant lifter, white fingerprint gelatin, black fingerprint gelatin, silicone, transparent adhesive tape, are suitable. Moreover, white fingerprint gelatin and white instant lifter proved to be very good at lifting treated finger marks. Black fingerprint gelatin was very good also, but finger marks were examined by slant light.     

The analysis of tire rubber traces collected after braking incidents using Pyrolysis-GasChromatography/Mass Spectrometry

Automobile tire marks can routinely be found at the scenes of crime, particularly hit-and-run accidents and are left on road surfaces because of sudden braking or the wheels spinning. The tire marks are left due to the friction between the tire rubber and the solid road surface, and do not always demonstrate the tire tread pattern. However, the tire mark will contain traces of the tire. In this study, Pyrolysis Gas Chromatography/Mass Spectrometry was used to analyze 12 tires from different manufacturer's and their traces collected after braking incidents. Tire marks were left on a conglomerate road surface with sudden braking. The samples were pyrolysed without removal of contaminant in a micro-furnace type pyrolyser. Quantitative and qualitative analysis were performed on all the samples. All 12 samples were distinguished from each other. Each of the tire traces were identified as coming from there original source.     

Fingerprint recovery from human skin surfaces.

A study was conducted to investigate whether certain dactyloscopic powders and reagents can recover latent fingerprints on human skin surfaces. Four fingerprint powders, Magnetic Jet Black, Magnetic Silver, Silver Special, Swedish Black, and two other methods, cyanoacrylate fuming (CA) and Ruthenium tetroxide (RTX), were used. Having examined skin surfaces with a forensic light source, we observed that the fingerprint impressions remained visible up to 15 min after intentionally placing them on the skin surface of living subjects and dead bodies. Finger marks were recovered and positive results were achieved with Magnetic Black and Swedish Black powder on living subjects. On dead bodies finger marks treated with cyanoacrylate were visible but those treated with RTX, Swedish Black and Magnetic Jet Black powder were useful for potential comparison. On dead bodies best results were obtained with RTX method.     

内、外铣槽钥匙机械配制痕迹的研究

目的研究内、外铣槽钥匙机械配制后痕迹的出现规律及其影响因素。方法利用传统的痕迹检验方法观察痕迹出现的位置、形态及分布规律。结果内、外铣槽钥匙机械配制后会留下不同于其原始加工痕迹和使用痕迹的增配痕迹，这种痕迹是否明显出现、出现的形态和位置受钥匙材质和结构、配匙机、配匙人员工作经验等因素的影响。结论当未发现内、外铣槽钥匙上有明显增配痕迹时，不能轻易做出钥匙未被增配的判断。     

The recovery of latent fingermarks and DNA using a silicone-based casting material

There are many techniques available for the recovery of fingermarks at scenes of crime including the possibility of taking casts of the marks. Casts can be advantageous in cases where other destructive recovery techniques might not be suitable, such as when recovering finger marks deposited on valued or immobile items. In this research, Isomark (a silicone-based casting material) was used to recover casts of finger marks placed on a variety of substrates. Casts were enhanced using cyanoacrylate fuming. Good quality marks were successfully recovered from a range of smooth, non-porous surfaces. Recovery from semi-porous surfaces was shown to be inefficient. DNA was subsequently extracted from the casts using QIAamp Mini extraction kits, amplified and profiled. Full DNA profiles were obtained 34% of samples extracted.     

Development of latent fingermarks on thermal paper: Preliminary investigation into use of iodine fuming

Thermal paper finds its extensive use in the modern day life and could act as a vital piece of physical evidence carrying latent fingermarks. A large number of citations are available in literature suggesting various techniques to develop these marks but all are suffering with one or the other drawbacks such as complex and cumbersome procedure, pre- or post-treatment, background coloration and efficiency to develop aged fingermarks. In present study, a very simple and novel method involving iodine fuming has been suggested to develop fingermarks which were not only permanent but also without any background coloration. The suggested method does not involve any pre- or post-treatment of the substrate and was able to develop very old fingermarks (upto >1 year). In this study an attempt has been made to explain the reaction mechanism of the process. In case of different types of thermal papers, presence of different substituents on leuco dye (lactone ring) structure resulted in development of different colored fingermarks upon reaction with iodine. Sebaceous material laden marks have been found to be more intensely developed as compared to eccrine marks, and the difference was more pronounced in case of aged fingermarks.     

Improve Toolmarks' Impressions in Soft Wax

When the forensic toolmarks laboratory receives for examination and comparison a tool that is suspected of having been involved in a crime, the expert performs tests designed to determine whether or not the specific tool generates the same toolmarks as those found at the crime scene. This is performed by testing tool striation on a piece of soft metal, such as lead, and examining the marks left by the tool. Studies have shown that wax may be an optimal material for this purpose. This study examines the use of wax at different temperatures and shows that quality of results is better when the wax is cooled (recommended temperature is ?18°C). At this temperature, the wax is flexible enough but does not smear and is not sticky. This makes the obtained marks clearer and of better quality.     

Chemical enhancement of footwear impressions in blood deposited on fabric — Evaluating the use of alginate casting materials followed by chemical enhancement

Most footwear marks made in blood on a surface such as fabric tend to be enhanced in situ rather than physically recovered using a lifting technique prior to enhancement. This work reports on the use of an alginate material to recover the impressed footwear marks made in blood and deposited on a range of fabric types and colours. The lifted marks were then enhanced using acid black 1 and leuco crystal violet with excellent results.This presents a new method for the lifting and recovery of blood impressions in situ from crime scene followed by subsequent mark enhancement of the lifted impression.     

A promising microbiological test for the diagnosis of drowning

A number of biological and chemical tests have been developed over the years to determine whether a person was drowned. This study focuses on the potential of a microbiological test for detecting common bacterial markers of water faecal pollution such as faecal coliforms (FC) and faecal streptococci (FS) as possible indicators of drowning. A promising previous study was carried out on central and peripheral blood samples of 42 drowned victims (20 cases in saltwater and 22 cases in freshwater) and 30 not-drowned bodies. To improve the accuracy of our previous results and also in order to investigate a possible cause of a false positive due to pulmonary passive diffusion and subsequently endogenous or exogenous bacterial invasion of the blood in the post-mortem interval (PMI), the FC and FS test was applied to bodies submerged in water but died from causes other than drowning. In the present study, blood samples collected from the left ventricle (LV), right ventricle (RV), femoral artery (FA) and, femoral vein (FV) of 10 drowned victims (5 cases in freshwater and 5 cases in seawater) and 3 not-drowned individuals with bodies submerged in water for a while after death have been analysed. Preliminary results are in agreement with other reports dealing with diatoms and marine bacteria that suggest to exclude the hypothesis of a passive penetration of sufficient quantities of drowning medium into circulation after death or during the agonal period. Based on our results there is also no evidence of a relevant dissemination of endogenous micro-flora from the gastrointestinal tract affecting the FS and FC test. There are still several other factors that could influence the applicability of post-mortem FS and FC cultures for the diagnosis of drowning and they need further investigations. The present article provides only a glimpse of the potential of the FS and FC test as bacteriological method for the diagnosis of drowning.     

Classification of firing pin impressions using HOG-SVM

Crimes, such as robbery and murder, often involve firearms. In order to assist with the investigation into the crime, firearm examiners are asked to determine whether cartridge cases found at a crime scene had been fired from a suspect's firearm. This examination is based on a comparison of the marks left on the surfaces of cartridge cases. Firing pin impressions can be one of the most commonly used of these marks. In this study, a total of nine Ruger model 10/22 semiautomatic rifles were used. Fifty cartridges were fired from each rifle. The cartridge cases were collected, and each firing pin impression was then cast and photographed using a comparison microscope. In this paper, we will describe how one may use a computer vision algorithm, the Histogram of Orientated Gradient (HOG), and a machine learning method, Support Vector Machines (SVMs), to classify images of firing pin impressions. Our method achieved a reasonably high accuracy at 93%. This can be used to associate a firearm with a cartridge case recovered from a scene. We also compared our method with other feature extraction algorithms. The comparison results showed that the HOG-SVM method had the highest performance in this classification task.     

Techniques for fingerprint recovery on vegetable and fruit surfaces used in Slovenia — A preliminary study

An examination was conducted to investigate whether certain dactyloscopic powders and reagents can recover latent fingerprints on vegetable and fruit surfaces (apple, banana, tomato and potato). Two fingerprint powders, Swedish Soot powder mixture (Swedish Black), Silver Special powder and cyanoacrylate fuming (CA), were investigated. The results have shown that detection with Swedish blackpowder is the most suitable procedure as the percentage finger marks which were of adequate quality for further examination, was higher than with any other technique examined.     

Comparative study of electrochromic enhancement of latent fingerprints with existing development techniques

To address the challenge of capturing latent fingerprint evidence from metal surfaces, a new method of latent fingerprint enhancement based on electrochromic polymer films has recently been developed. Here, we present a study comparing the development and visualization of nonvisible fingerprints on stainless steel substrates using this electrochromic enhancement approach with three classical methods (dusting, wet powder, and cyanoacrylate fuming). Two variants of the electrochromic enhancement method were utilized with polyaniline and poly(3,4-ethylenedioxythiophene) as the electrochromic materials. Fingerprint samples were taken from different donors (varying in age and gender) and were exposed to different environments for systematically varied periods of time (up to 28 days). The environments represent plausible evidential scenarios: left under ambient conditions, washed with aqueous soap solution, washed with acetone, submerged in water, and maintained at elevated temperature. The electrochromic enhancement procedure frequently outperformed the traditional methods, particularly for samples exposed to more challenging histories.     

Comparison of Dimensional Accuracies Using Two Elastomeric Impression Materials in Casting Three‐dimensional Tool Marks

The purpose of this study was to evaluate two types of impression materials which were frequently used for casting three‐dimensional tool marks in China, namely (i) dental impression material and (ii) special elastomeric impression material for tool mark casting. The two different elastomeric impression materials were compared under equal conditions. The parameters measured were dimensional accuracies, the number of air bubbles, the ease of use, and the sharpness and quality of the individual characteristics present on casts. The results showed that dental impression material had the advantage of special elastomeric impression material in casting tool marks in crime scenes; hence, it combined ease of use, dimensional accuracy, sharpness and high quality.     

Detection of "uncommon" tranquillizers-sedatives during screening toxicological analysis

A 56-year-old man is discovered unconscious in a pool of blood in the kitchen of his house. According to findings, the man used a 22 long Rifle to fire 14 shots at his thorax with trajectories going from front to back, from right to left and on a nearly horizontal level. All the projectiles got into the left front side of his thorax and came out just under the back of his left armpit. One of them then got through his left arm and fractured his left humerus. According to the findings made on the premises and the position of the bloodstains, we think that man put his rifle against the wall, resting on a pipe. He fired, unloading two clips into his thorax. He had to handle the bolt of the rifle before each shot. To reload, he took the bullets which were on the nearby table on which blood marks can be seen. When reloading at a certain moment, he sat down in his armchair and when he wanted to stand up, he leaned on the armrests, on which blood marks can be seen. The last bullet was probably the one which went through his left arm, preventing him from keeping on shooting. His death, caused by a hypovolemical shock, was obviously very slow.     

Determining an Optimal Sequence for Chemical Development of Latent Prints on Cartridge Casings and Shotgun Shells*,†

Abstract: In developing latent prints on cartridge casings and shotgun shells, multiple chemical processes should be used in order to obtain the best results. In Phase I, this study established an optimal chemical sequence for both Brass and Nickel cartridge casings based on six sequences involving four chemicals: Cyanoacrylate, Black Powder, Rhodamine 6G and Acidified Hydrogen Peroxide. Phase II was a validation study of Phase I involving a random sample of both Brass and Nickel cartridge casings, which were processed according to the determined optimal sequences. In addition, ribbed shotgun shells were processed under Phase I results and determined to be dependent upon the utilization of a CrimeScope at 515 nm. Consideration should be given to the type of cartridge case being examined. Although limitations exist, some chemical sequences undeniably work better than others. All photographs were manipulated with Adobe^® Photoshop^®. All results were verified by a senior latent print examiner.     

Detection of nitro-organic and peroxide explosives in latent fingermarks by DART- and SALDI-TOF-mass spectrometry

The ability of two mass spectrometric methods, surface-assisted laser desorption/ionization-time of flight-mass spectrometry (SALDI-TOF-MS) and direct analysis in real time (DART-MS), to detect the presence of seven common explosives (six nitro-organic- and one peroxide-type) in spiked latent fingermarks has been examined. It was found that each explosive could be detected with nanogram sensitivity for marks resulting from direct finger contact with a glass probe by DART-MS or onto stainless steel target plates using SALDI-TOF-MS for marks pre-dusted with one type of commercial black magnetic powder. These explosives also could be detected in latent marks lifted from six common surfaces (paper, plastic bag, metal drinks can, wood laminate, adhesive tape and white ceramic tile) whereas no explosive could be detected in equivalent pre-dusted marks on the surface of a commercial lifting tape by the DART-MS method due to high background interference from the tape material. The presence of TNT and Tetryl could be detected in pre-dusted latent fingermarks on a commercial lifting tape for up to 29 days sealed and stored under ambient conditions.     

Dynamics of latent fingerprints: The effect of physical factors on quality of ninhydrin developed prints — A preliminary study

The conditions under which latent fingerprints are deposited affect the process of development that can be used to effectively recover these marks. The conditions which can play a part include environmental conditions, the type of surface on which latents are deposited, the ability of the donor to deposit fingerprints, contact time, force of contact with the object etc. Very little previous work is available in the scientific literature addressing these conditions and therefore, an attempt has been made in this present study to assess the effect of some of these criteria and their effect on the ability of ninhydrin to develop the marks. Latent fingerprints from good and bad donors were obtained on paper with variable pressure under controlled conditions. Laboratory prepared 1% ninhydrin solution was used to visualise the prints.     

Cooling rates of the ear and brain in pig heads submerged in water: implications for postmortem interval estimation of cadavers found in still water

The state of the art for determining postmortem interval in submerged bodies reflects a serious lack of studies. The objectives of the present study were therefore to study cerebral and tympanic cooling in water and its relation to cooling in air, in a pig model. First of all, cerebral and tympanic cooling on a single head and on an entire body were compared and proven to be very similar in air and in water. Nine pairs of heads were then exposed to 9 temperature intervals from 0 degrees C to 20 degrees C. For every set temperature, one head was placed in water, the other in "ambient" air in a thermostatic chamber. Ear and brain temperature were simultaneously measured every 10 minutes during 8 hours. Results showed that both in air and in water, cooling curves were almost exponential, regardless of the site (ear or brain) or the environmental temperature. Cooling was always more rapid in water than in air. Cerebral and tympanic cooling always had a correlation coefficient of 0.98-0.99. Assuming that these cooling patterns are applicable to man, this research may provide a starting point for postmortem interval estimation in submerged cadavers.     

通过痕迹认定肇事车辆

随着交通事故勘验技术的发展,物证技术在重特大交通事故现场勘验以及侦破交通逃逸案件中发挥的作用越来越重要.痕迹检验技术作为物证技术的一个重要分支,在认定肇事车辆中发挥着举足轻重的作用.交通事故中的痕迹是车辆与车辆、人体、道路等客体在路面上相对高速运动形成的痕迹,相对于其它类型案件有着自己的特点.交通事故中的痕迹分布范围广、造痕体和承痕体相对运动剧烈,形成痕迹的造痕体和承痕体大多都会发生形变.基于交通事故中痕迹形成的这些特点,交通事故中的痕迹检验难度是比较大的.但交通事故中车辆的特殊结构形成的印压痕迹、车辆轮胎、摩托车车篮等造痕体在灰尘等介质作用下在人体的衣服等表面形成的印压痕迹都可以很好反映造痕体的外部结构特征,从这些痕迹反映出造痕体的外部结构特征可以寻找和认定交通肇事车辆.