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Strelova OIu Vozheva AB Slonimskaia EA Strelkova LF 《Sudebno-meditsinskaia ekspertiza》2007,50(3):31-33
The authors present a method of hingamine identification in non-biological substances (tablets, powder, syringes) and biological fluids (blood, urine). Isolation was made with chloroform in pH 10. Identification was conducted with thin-layer chromatography, gas chromatography/mass-spectrometry, high-performance liquid chromatography, spectrophotometry in UV region. The quantity was estimated with spectrophotometry in UV region, high-performance liquid chromatography and high-performance thin-layer chromatography. The results of the three methods are comparable. 相似文献
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Kireeva AV Vozheva AB Bakhtina SM Volchenko SV Kuklin VN 《Sudebno-meditsinskaia ekspertiza》2007,50(3):22-25
The conditions of doxilamine isolation from biological fluids are studied. The method of its extraction with a mixture of organic solvents in pH 9 is proposed. Identification of doxilamine with techniques of thin layer chromatography, UV-, IR-spectroscopy, chromato-mass-spectrometry, densitometry, gas-liquid chromatography is described. UV-spectrometry, gas chromatography and densitometry can be used for quantitation of doxilamine. 相似文献
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