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131.
132.
Eckenrode BA Ramsey SA Stockham RA Van Berkel GJ Asano KG Wolf DA 《Journal of forensic sciences》2006,51(4):780-789
The Scent Transfer Unit (STU-100) is a portable vacuum that uses airflow through a sterile gauze pad to capture a volatiles profile over evidentiary items for subsequent canine presentation to assist law enforcement personnel. This device was evaluated to determine its ability to trap and release organic compounds at ambient temperature under controlled laboratory conditions. Gas chromatography-mass spectrometry (GC-MS) analyses using a five-component volatiles mixture in methanol injected directly into a capture pad indicated that compound release could be detected initially and 3 days after the time of collection. Additionally, 15 compounds of a 39-component toxic organic gaseous mixture (10-1000 parts per billion by volume [p.p.b.(v)]) were trapped, released, and detected in the headspace of a volatiles capture pad after being exposed to this mixture using the STU-100 with analysis via GC-MS. Component release efficiencies at ambient temperature varied with the analyte; however, typical values of c. 10% were obtained. Desorption at elevated temperatures of reported human odor/scent chemicals and colognes trapped by the STU-100 pads was measured and indicated that the STU-100 has a significant trapping efficiency at ambient temperature. Multivariate statistical analysis of subsequent mass spectral patterns was also performed. 相似文献
133.
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135.
Vincent?B.?Van HasseltEmail author John?J.?Flood Stephen?J.?Romano Gregory?M.?Vecchi Nathalie de?Fabrique Vincent?A.?Dalfonzo 《Journal of family violence》2005,20(1):21-27
Initial reports of domestic violence are generally made to law enforcement officers who must respond and intervene. A subset of these episodes involves cases in which the victim, and, in many instances her child(ren), have been taken hostage by her husband or partner. Moreover, there are indications that the number of such incidents is growing. The purpose of this project was twofold: (1) to provide one of the first reports on the prevalence and characteristics of these events, and (2) to more closely analyze domestic crisis (hostage) situations using actual case examples. All information was obtained from the Hostage Barricade Database System (HOBAS) of the FBIs Crisis Negotiation Unit. HOBAS is a postincident information collection tool which stores historical data from law enforcement agencies across the nation on hostage/barricade incidents. An examination of this database yielded different types of domestic hostage-taking acts and outcomes (e.g., tactical vs. negotiated resolutions, survival vs. death/injury of perpetrator and/or victim[s]). Implications of the findings, for future crisis negotiation efforts directed toward nonviolent resolution of these high-risk critical incidents, are discussed. 相似文献
136.
This article based, on 38 in-depth interviews with Rotterdam cocaine retail dealers, aims to present a clearer picture of
how cocaine supply lines in the Netherlands are organized in order to fine-tune policy with respect to crime, public order
and safety on the different trade levels. On the retail level the market for cocaine is strictly separated in a market for
crack cocaine versus a market for powder cocaine. The crack dealers are often hard drug users themselves living in relatively
poor circumstances. Although dealing cocaine is their main activity, they tend to be involved in other activities related
to the drug scene, e.g. smuggling cocaine via Amsterdam airport. The cocaine distribution line for supply on the local market
is seldom more than two steps. Because the supply for the Rotterdam cocaine retailers comes mainly from small-scale imports,
successful police operations against large-scale imports of cocaine will have little influence on the local cocaine supply
in the Netherlands. 相似文献
137.
Lock E Aalberg L Andersson K Dahlén J Cole MD Finnon Y Huizer H Jalava K Kaa E Lopes A Poortman-van der Meer A Sippola E 《Forensic science international》2007,169(1):77-85
This paper is the fifth in a series of six in relation to the development of a harmonised method for the profiling of amphetamine [L. Aalberg, K. Andersson, C. Bertler, H. Borén, M.D. Cole, J. Dahlén, Y. Finnon, H. Huizer, K. Jalava, E. Kaa, E. Lock, A. Lopes, A. Poortman-van der Meer, E. Sippola, Development of a harmonised method for the profiling of amphetamines I. Synthesis of standards and compilation of analytical data, Forensic Sci. Int. 149 (2005) 219-229; L. Aalberg, K. Andersson, C. Bertler, M.D. Cole, Y. Finnon, H. Huizer, K. Jalava, E. Kaa, E. Lock, A. Lopes, A. Poortman-van der Meer, E. Sippola, J. Dahlén, Development of a harmonised method for the profiling of amphetamines II. Stability of impurities in organic solvents, Forensic Sci. Int. 149 (2005) 231-241]. The third paper [K. Andersson, K. Jalava, E. Lock, L. Aalberg, Y. Finnon, H. Huizer, E. Kaa, A. Lopes, A. Poortman-van der Meer, M.D. Cole, J. Dahlén, E. Sippola, Development of a harmonised method for the profiling of amphetamines III. Development of the gas chromatographic method, Forensic Sci. Int., in press] dealt with the optimisation of the gas chromatographic and detection methods whereas the fourth paper [K. Andersson, K. Jalava, E. Lock, Y. Finnon, S. Stevenson, L. Aalberg, H. Huizer, E. Kaa, A. Lopes, A. Poortman-van der Meer, M.D. Cole, J. Dahlén, E. Sippola, Development of a harmonised method for the profiling of amphetamines IV. Optimisation of sample preparation, Forensic Sci. Int., in press] concerned the optimisation of the extraction method prior to GC analysis. This paper is a study of the optimised method in order to determine its stability. Investigations of within and between day variations were carried out in four laboratories. Moreover, variations between laboratories were also determined. Both flame ionisation detector (FID) and MS detection were used. One laboratory studied nitrogen-phosphorous detector (NPD) detection as well. For this task, 12 batches of amphetamine were prepared. Six of them were synthesised via the Leuckart route, three via the nitrostyrene route and three via the reductive amination route [A.M.A. Verweij, Impurities in illicit drug preparations: amphetamine and methamphetamine, Forensic Sci. Rev. 1 (1989) 2-11]. Taking into account all studied target compounds and the average results from four laboratories, the within day variation was around 6% for FID and 5% for MS, the between days variation was around 10% for FID and 8% for MS. For NPD detection, within day variation was 5% and between days variation 9% (only one laboratory). Finally, the inter-laboratory variation was about 12% for FID (four laboratories) and 10% for MS (three laboratories). 相似文献
138.
This study investigates media priming effects in the context of a Summit meeting of European Union (EU) leaders. It differs
in four ways from most previous non-experimental priming studies: (1) it provides survey data accompanied by a content analysis
of the news, (2) it compares priming effects on evaluations of a number of political leaders, who differed in their visibility
in the news, (3) it involves an issue with low salience, and (4) it studies priming effects in the context of a European Parliamentary
democracy. The study involves a two-wave panel study (before and after the Summit) on a representative sample of 817 Dutch
adults, and a content analysis of the newspaper and television news in the 8 weeks leading up to the Summit meeting. The study
shows that media priming effects occur only for the politicians who appeared visible in the news in connection with the issue.
The media priming effects were not significantly moderated by political attentiveness or by political knowledge. We also explore
the aggregate level consequences of priming for the popularity of leaders, and demonstrate that, as a result of media priming,
two politicians became more popular, despite having received a bad press.
相似文献
Wouter van der BrugEmail: |
139.
In Opinion 1/2010, the Article 29 Data Protection Working Party has provided additional guidance concerning the concepts of ‘controller’ and ‘processor’ contained in Directive 95/46/EC. This guidance aims to assist practitioners in their determination of whether an entity is acting as a controller or as a processor towards a particular data processing operation. Despite the fact that this opinion is informative, the existing framework still appears to leave room for a considerable amount of legal uncertainty. This uncertainty is attributable in part to the nature of the existing concepts, but also (and perhaps to a larger extent) to their apparent misalignment with current processing realities. In this paper, the author seeks to articulate why the existing concepts often remain difficult to apply in practice, in order to enable a constructive reflection on how these issues might be addressed in the future. 相似文献
140.
Ted Palmer Patricia Van Voorhis Faye S. Taxman Doris L. MacKenzie 《Journal of Experimental Criminology》2012,8(2):103-115