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Francesco Saverio Romolo Melanie J. Bailey Janella de Jesus Luigi Manna Matteo Donghi 《Science & justice》2019,59(2):181-189
Gunshot Residue (GSR) produced by the discharge of a firearm often provides very useful information in criminal investigations in cases involving the use of firearms. Scanning Electron Microscopy equipped with an Energy Dispersive X-ray Spectrometer (SEM-EDS) is typically used worldwide to visualize micrometric particles constituting GSR and to analyse their elemental composition. The 2017 ASTM Standard guide for gunshot residue analysis by scanning electron microscopy/energy dispersive X-ray spectroscopy specifies that “Particles classified as characteristic of GSR will have one of the following elemental compositions: Lead, antimony, barium; Lead, barium, calcium, silicon, tin”. For the first time, the presence of an additional element, such as Sn, plays a key role in ASTM particle classification. It is known that some ammunitions, used for pistols, revolvers and rifles, contain tin foil discs for sealing the primer mixture into the cup, resulting in GSR particles containing Sn. The authors faced some cases in which Sn was unexpectedly found in GSR particles from a 0.22 Long Rifle derringer and from some 12 gauge shotguns. No tin foil discs are used in rimfire ammunitions and there is no published evidence of tin foil discs in shotshell ammunitions. Following a “case by case” approach, experimental research has been carried out to explain how Sn can be present in GSR particles when the last discharged cartridge also does not contain any Sn either in components and in the explosive charges.Moreover, the use of Particle Induced X-ray Emission (PIXE) showed the capability to overcome overlap ambiguity of Sb and Sn peaks in the X-ray spectra, being a possible key issue in real shooting cases if Sn quantities are below the lower limit of SEM detection, especially when Sb is also present. 相似文献
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Elena Pilli Silvia Boccone Alessandro Agostino Antonino Virgili Giancarlo DErrico Martina Lari Cesare Rapone Filippo Barni Jacopo Moggi Cecchi Andrea Berti David Caramelli 《Science & justice》2018,58(6):469-478
During the Second World War, on 24th March 1944, 335 Italians were massacred near Rome by the occupying forces of Nazi Germany. Four months later forensic examination led to the identification of 323 out of 335 victims. After approximately 60?years, the identification of the remaining unidentified twelve victims began with anthropological and genetic analysis carried out by a team of Italian forensic experts. Anthropological analysis was performed in field in order to confirm the sex of each victim and verify the presence of only one individual in each grave for a correct sampling. Selected bone fragments for each individual were then collected and transferred to the laboratory for genetic analysis. Although the anthropological ante mortem information was limited, morphological and metrical data was collected for a possible future identification of the victims. Subsequently, the typing of autosomal loci, Y-STR and mtDNA D-loop region of all bone and available reference samples was conducted. LR and cumulative LRs obtained from autosomal STR and Y-STR results confirmed the alleged relationship between three victims and their relatives with values over 104 (one sample) and 106 (two samples). Therefore, the genetic analysis offered the families the possibility of replacing the number of the grave with the name of the victim. 相似文献
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Harald Winkler Niklas Höhne Guy Cunliffe Takeshi Kuramochi Amanda April Maria Jose de Villafranca Casas 《International Environmental Agreements: Politics, Law and Economics》2018,18(1):99-115
In the lead-up to the Paris Agreement, every country was invited to submit an intended nationally determined contribution (INDC), and indicate how it is fair. We analyse how countries have explained the equity of mitigation and adaptation in 163 INDCs, providing a bottom-up analysis of equity to complement a literature that has focused on top-down allocations. While no single indicator of equity was used by all INDCs, a menu of quantified indicators or tiered approaches could provide bounded flexibility across different national circumstances. The most common equity indicator used in mitigation INDCs is the country’s ‘small share’ of global emissions, followed by per capita emissions. The emissions of individual ‘small share’ INDCs add up to 24% of annual global emissions when using a consistent data set. Per capita emissions are used across a range of countries with low (0.5) to high (25 t CO2–eq per capita) values for that indicator. Adaptation is included in 89% of INDCs, of which more than half quantify impacts in some manner, and two-thirds use vulnerability as an equity argument. Broadly, we find that most claims to equity are either unsubstantiated or drawn from analysis by in-country experts. Only two INDCs refer to independent evidence, and none consider the consequences of their approach when applied to all countries. Given that the aggregate effect of INDCs will not be sufficient to keep global temperature increase well below 2 °C, and even less to keep temperature below a 1.5 °C rise, the INDCs have distributional implications. More rigorous information is needed to assess relative fair shares, which could be provided officially in future nationally determined contributions (NDCs). Absent improved information, it is likely that researchers and civil society will continue to assess informally what could be considered fair. A hybrid approach to equity—combining bottom-up assessment and top-down allocation—would be consistent with the hybrid architecture of the Paris Agreement, which comprises bottom-up elements such as NDCs and top-down elements such as global goals. Improved information on equity in NDCs will be an important input to the global stocktake ‘in the light of equity’. 相似文献
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Traditional research on community awareness and use of sex offender registries relies upon random digit dialing and other survey instruments. While important sources of data, these sources have limitations and attempts to improve on these measures are bound to funding limitations impeding the collection of larger samples. Analyzing internet search query data associated with interest in sex offender registries from 2006–2016, we explore regional and temporal trends associated with interest in sex offender registries. Results substantiate prior research using mail and telephone surveys, and that of other similar methodologies, showing that interest in sex offender registries display low to moderate interest, which are relatively stable overtime and declining in interest. 相似文献
996.
巴西--发展中大国及其国际战略 总被引:3,自引:2,他引:1
路易斯·奥古斯托·德卡斯特罗·内维斯 《拉丁美洲研究》2005,27(5):54-57
这是本刊增设的一个栏目。顾名思义,“大使论坛”就是大使们的论坛。它是由中国社会科学院国际合作局与社科院其他研究所主办的一个论坛,而2005年8月18日由中国社会科学院国合作局和拉美所主办的“巴西的大国地位与大国战略”是首届大使论坛。在首届大使论坛上,巴西驻中国大使路易斯·奥古斯托·德卡斯特罗·内维斯先生作了题为《巴西———发展中大国及其国际战略》的报告并回答了与会者提出的问题。 相似文献
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POPULATION: Over 259 unrelated individuals from the State of Sergipe (Northeastern Brazil). 相似文献