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A method for detection and quantification of 21 benzodiazepines and the pharmacologically related "z-drugs" in human hair samples was developed and fully validated using liquid chromatography coupled to tandem mass spectrometry (LC-MS/MS). After methanolic and methanolic/aqueous extraction, the analytes were separated using two different LC-MS systems (AB Sciex 3200 QTRAP and AB Sciex 5500 QTRAP). Separation columns, mobile phases and MS modes for both systems were: Phenomenex Kinetex, 2.6 μm, 50/2.1; 5mM ammonium formate buffer pH 3.5/methanol, total flow 0.75 mL/min; electrospray ionization (ESI), multiple reaction monitoring (MRM), information dependent acquisition (IDA), enhanced product ion scan (EPI). The assays were found to be selective for the tested compounds (alprazolam, 7-aminoclonazepam, 7-aminoflunitrazepam, bromazepam, chlordiazepoxide, clonazepam, N-desalkylflurazepam, diazepam, flunitrazepam, flurazepam, alpha-hydroxymidazolam, lorazepam, lormetazepam, midazolam, nitrazepam, nordazepam, oxazepam, phenazepam, prazepam, temazepam, triazolam, zaleplon, zolpidem and zopiclone), all validation criteria were in the required ranges according to international guidelines, except for bromazepam. Matrix effects, and process efficiencies were in the acceptable ranges evaluated using the post-extraction addition approach. Lower limits of quantification were between 0.6 and 16 pg/mg of hair. The LC-MS/MS assay has proven to be applicable for determination of the studied analytes in human hair in numerous authentic cases (n=175). 相似文献
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Kristina Jerre 《European Journal on Criminal Policy and Research》2014,20(1):121-136
Public opinion has come to be given an increasingly important role in the crime policy debate of western countries. The task of problematising different pictures that emerges from different studies of public opinion on appropriate sentences thus becomes an important task. In this article the question is whether survey respondents, in their choice of reactions to crime, tend to propose shorter prison sentences when they combine the prison term with other measures? If so, different response instructions can lead to different conclusions as to what survey participants consider to be appropriate sentences. Earlier research points at such tendencies to some extent. In order to examine this question, two comparisons will be made. In the first, survey respondents who chose to combine a prison sentence with other measures is compared with those who chose to propose a prison sentence as the only sanction. In the second, participant who were instructed to only propose a single sanction will be compared with those who were given the opportunity to combine two sanctions. Both comparisons are made with regard to the lengths of the proposed prison sentences. No systematic differences emerge. The correlation between the length of prison term proposed and the choice, or opportunity given, to combine the prison term with other measures varies, for example, across the different offences examined. The choice of appropriate reactions to crime is based on a more advanced deliberation than whether different sanctions may be combined. 相似文献
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Turning defiance into compliance with procedural justice: Understanding reactions to regulatory encounters through motivational posturing
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Kristina Murphy 《Regulation & Governance》2016,10(1):93-109
This paper uses Braithwaite's motivational posturing framework to explain how individuals react to encounters with regulatory authorities. Of interest is whether procedural justice can reduce defiance and improve self‐reported compliance among individuals who are either resistant or dismissive of regulatory authority. Using longitudinal survey data collected from tax offenders (Study 1), and individuals who had a recent police‐citizen interaction (Study 2), it will be shown that procedural justice can promote compliance behavior. Procedural justice is also found to be effective for reducing resistant forms of defiance over time, but not dismissive defiance. Further, the results reveal that neither resistant defiance nor dismissive defiance moderate the effect of procedural justice on compliance, suggesting procedural justice works equally well for both low and high resisters and low and high disengagers. Finally, an unexpected result reveals that resistance, but not dismissive defiance, mediates the effect of procedural justice on self‐reported compliance behavior. The findings have implications for procedural justice research and for the regulation of defiance. 相似文献
15.
The heightened threat of terrorism in the West has resulted in more power being granted to police. However, new anti-terror laws and heavy-handed policing practices can stigmatize Muslim communities. Using survey data from 800 Australian Muslims this paper examines whether procedural justice policing in counter-terrorism enhances Muslims’ feelings of social inclusion, and promotes their intentions to report terror threats to police. Of interest is how procedural justice influences Muslims who feel less socially included. Three competing theoretical frameworks differ in the predictions they make about when and why procedural justice influences excluded groups. This paper considers each framework and discusses how each explains the relationships between our variables of interest. Our findings show that procedural justice is positively associated with social inclusion and intentions to report terror threats to police. Findings also show that social inclusion both moderates and partially mediates the effect of procedural justice on reporting intentions. 相似文献
16.
When Free Traders Become Protectionists: Constituent Advocacy at the International Trade Commission
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Although Members of Congress vote on few trade bills, they participate regularly in venues such as the International Trade Commission (ITC), where important trade policy decisions are made. We assert that once removed from the voting chambers of Congress, legislators are motivated overwhelmingly by the desire to advance constituents’ trade policy interests, even those that contradict the member’s established positions on trade. Utilizing an original dataset on legislator participation in antidumping cases, we find that both Democratic and Republican members advocate protection at the ITC when they have numerous firms and constituents in their district who benefit from trade restrictions, particularly when they receive sizeable financial contributions from them. Notably, self‐proclaimed free‐traders are just as likely to seek protection for their constituents as are trade opponents. Away from Capitol Hill, then, trade policymaking exhibits few partisan and ideological influences and serves as a means for members to expand political support. [Correction added on 21 August 2018, after first online publication: Abstract was added to article] 相似文献
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Research consistently finds that if authorities use procedural justice in encounters with the public then this will promote citizen cooperation and compliance with the law. Recently, the importance of people's emotional reactions in response to procedural justice and injustice, and the subsequent effect this has on behaviour have been examined. This paper utilises a multi-method approach to examine the mediating role that negative affect plays in the effect of procedural justice policing on citizen compliance behaviour. Study 1 utilises both cross-sectional and longitudinal field survey data collected from Australian citizens who have had a recent contact with a police officer. Study 2 utilises an experimental vignette study designed to assess the causal mechanisms involved in the procedural justice–emotion–compliance relationship. Both studies find that procedural justice is linked to people's self-reported propensity to comply with police. Study 1 and 2 also find that negative affect mediates this relationship. These findings have important implications for training police to interact with the public in a manner that reduces negative emotions and ensures the highest level of compliance from the public. 相似文献
19.
This paper addresses new challenges and identifies starting points for development theory following recent debates in Latin America on ‘new or neo-extractivism’. It focuses on the concept of neo-extractivism and the context of its emergence, and on the changing role of the state. Looking at a number of social economic indicators, we find that, even after considering differences between countries, (neo-)extractivism is not merely a temporary economic strategy in the region. Instead, it exhibits features of a consolidated development project. Empirical evidence from the region shows the fundamental implications of resource-based development paths in politics, social relations and territorial orders. To grasp these implications conceptually, we argue for a shift in theoretical perspectives related to the link between development and resource extraction. Key elements for such a shift are to be found in recent studies in rentier theory and politics and new approaches in the field of political ecology. 相似文献
20.
Drawing on a representative sample of four countries, this article compares two related aspects of interest group activity across Latin America. First, it identifies the elements that determine the level of interest group system development and types of group activity across the region; and second it provides insights into the relationship of the level of institutionalization of a group system to the extent of the consolidation of democracy. The representative sample is composed of Uruguay and Costa Rica in comparison with Paraguay and Haiti. These are four countries with small populations that cover the spectrum of levels of socioeconomic and political development across Latin America, from Uruguay, one of the most developed, to Haiti one of the least developed. The article argues that across a spectrum of group development in Latin America, advanced systems have more or less integrated characteristics, whereas less developed ones manifest a dual or bifurcated group activity. Copyright © 2014 John Wiley & Sons, Ltd. 相似文献