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921.
Determination of Herbicides Paraquat,Glyphosate, and Aminomethylphosphonic Acid in Marijuana Samples by Capillary Electrophoresis 下载免费PDF全文
Rafael Lanaro M.Sc. José L. Costa Ph.D. Silvia O. S. Cazenave Ph.D. Luiz A. Zanolli-Filho M.Sc. Marina F. M. Tavares Ph.D. Alice A. M. Chasin Ph.D. 《Journal of forensic sciences》2015,60(Z1):S241-S247
In this work, two methods were developed to determine herbicides paraquat, glyphosate, and aminomethylphosphonic acid (AMPA) in marijuana samples by capillary electrophoresis. For paraquat analysis, sample was extracted with aqueous acetic acid solution and analyzed by capillary zone electrophoresis with direct UV detection. The running electrolyte was 50 mmol/L phosphate buffer (pH 2.50). For glyphosate and AMPA, indirect UV/VIS detection was used, as these substances do not present chromophoric groups. Samples were extracted with 5 mmol/L hydrochloric acid. The running electrolyte was 10 mmol/L gallic acid, 6 mmol/L TRIS, and 0.1 mmol/L CTAB (pH = 4.7). The methods presented good linearity, precision, accuracy, and recovery. Paraquat was detected in 12 samples (n = 130), ranging from 0.01 to 25.1 mg/g. Three samples were positive for glyphosate (0.15–0.75 mg/g), and one sample presented AMPA as well. Experimental studies are suggested to evaluate the risks of these concentrations to marijuana user. 相似文献
922.
The Effects of Dextromethorphan on Driving Performance and the Standardized Field Sobriety Test 下载免费PDF全文
Paul J. Perry B.Pharm. Ph.D. Kristian Fredriksen B.A. Stephanie Chew B.A. Eric J. Ip Pharm.D. Ingrid Lopes D.O. Shadi Doroudgar Pharm.D. Kelan Thomas Pharm.D. M.S. 《Journal of forensic sciences》2015,60(5):1258-1262
Dextromethorphan (DXM) is abused most commonly among adolescents as a recreational drug to generate a dissociative experience. The objective of the study was to assess driving with and without DXM ingestion. The effects of one‐time maximum daily doses of DXM 120 mg versus a guaifenesin 400 mg dose were compared among 40 healthy subjects using a crossover design. Subjects’ ability to drive was assessed by their performance in a driving simulator (STISIM® Drive driving simulator software) and by conducting a standardized field sobriety test (SFST) administered 1‐h postdrug administration. The one‐time dose of DXM 120 mg did not demonstrate driving impairment on the STISIM® Drive driving simulator or increase SFST failures compared to guaifenesin 400 mg. Doses greater than the currently recommended maximum daily dose of 120 mg are necessary to perturb driving behavior. 相似文献
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924.
Genetic Privacy 总被引:1,自引:0,他引:1
Lawrence O. Gostin 《The Journal of law, medicine & ethics》1995,23(4):320-330
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