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Analytical method for the determination of strychnine in tissues by gas chromatography/mass spectrometry: two case reports 总被引:4,自引:0,他引:4
Marques EP Gil F Proen"ca P Monsanto P Oliveira MF Castanheira A Vieira DN 《Forensic science international》2000,110(2):145-152
This paper describes an analytical method for strychnine determination in biological samples by gas chromatography/mass spectrometry and their application in the investigation of two cases involving strychnine ingestion: A fatal case and a clinical one. The strychnine is isolated from biological samples using a liquid-liquid extraction procedure. The clean-up procedure is performed using an acid solution. Papaverine is used as internal standard in the quantification of strychnine. In the analysed specimens, the limits of quantification were 0.1 microg/ml or 0.1 microg/g. The recovery rate ranged from 75.0% to 98.7% and the coefficients of variation ranged from 4.8% to 10.5%. 相似文献
23.
We describe a procedure for reconstructing documents that have been shredded by hand, a problem that often arises in forensics. The proposed method first applies a polygonal approximation in order to reduce the complexity of the boundaries and then extracts relevant features of the polygon to carry out the local reconstruction. In this way, the overall complexity can be dramatically reduced because few features are used to perform the matching. The ambiguities resulting from the local reconstruction are resolved and the pieces are merged together as we search for a global solution. The preliminary results reported in this paper, which take into account a limited amount of shredded pieces (10-15) demonstrate that feature-matching-based procedure produces interesting results for the problem of document reconstruction. 相似文献
24.
Iwamura ES Oliveira CR Soares-Vieira JA Nascimento SA Muñoz DR 《The American journal of forensic medicine and pathology》2005,26(1):33-44
Forensic identification of human remains is composed of anthropological study of race, sex, age, etc. By using these traditional methods, inconclusive or nonidentified cases could be subjected to DNA analysis. However, in spite of advances in human identification techniques, especially by PCR-amplified DNA, some limitations that affect the ability of obtaining DNA from human remains still persist. Light microscope sections of postmortem compact bones from human remains are presented here for the purpose of increasing a forensic examiner's prediction of successful nuclear DNA typing. Femoral compact bones were obtained from 7 human remains found on the ground, in different degrees of decomposition, and were cleaned by boiling to remove soft tissues, 8 collections of bones having undergone natural decomposition, not boiled (as no soft tissue was adhered), and 5 cadavers 12 to 16 hours postmortem. The histologic sections were stained by hematoxylin and eosin, the loci CSF1PO, TPOX, TH01, F13A01, FESFPS, vWA, D16S539, D7S820, D13S317, and amelogenin were amplified by PCR, and the polyacrylamide gel was stained with silver. The results presented here clarify questions concerning the viability of DNA for identification analysis, and they also may help to establish better strategies for optimization of DNA extraction and analysis in compact bones of human remains. 相似文献
25.
International legal scholars have identified and argued for and against new forms of non-consent-based international law. We study variation in Brazilian public opinion about adherence to international law created in three different ways: through a consent-based multilateral treaty, by the U.N. Security Council with the participation of Brazil, and by the U.N. Security Council without the participation of Brazil. Information that Brazil has participated in creating the international legal obligation through a multilateral treaty or membership on the Security Council yields levels of support for adherence to the legal obligation that are similar to those found when the origins of the legal obligation are generic. Information that the international legal obligation was created without Brazil’s participation, on the other hand, results in reduced support for compliance. This difference, which is particularly concentrated among highly educated respondents, is not driven by reduced concerns about reputational consequences or sanctions. Our results suggest that the increased use of non-consent-based forms of international law might be challenged by a lack of public support for compliance. 相似文献
26.
In 2003, the Workers’ Party took federal office in Brazil on an agenda of social inclusion and popular participation. This paper explores attempts to implement that agenda in big infrastructure projects in the Amazon: the BR-163 road and the Belo Monte dam. We argue that overlapping inequalities (between social groups, within the bureaucracy and between territorial centre and periphery) result in uneven state capacities for implementing projects in the Amazon. This framework helps explain why the government has moved much faster in building infrastructure than in implementing participatory social and environmental programmes that would benefit affected local communities. 相似文献
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Soy has become one of the world's most important agroindustrial commodities – serving as the nexus for the production of food, animal feed, fuel and hundreds of industrial products – and South America has become its leading production region. The soy boom on this continent entangles transnational capital and commodity flows with social relations deeply embedded in contested ecologies. In this introduction to the collection, we first describe the ‘neo-nature’ of the soy complex and the political economy of the sector in South America, including the new corporate actors and financial mechanisms that produced some of the world's largest agricultural production companies. We then discuss key environmental debates surrounding soy agribusiness in South America, challenging especially the common arguments that agroindustrial intensification ‘spares land’ for conservation while increasing production to ‘feed the world’. We demonstrate that these arguments hinge on limited data from a peculiar portion of the southern Amazon fringe, and obfuscate through neo-Malthusian concerns multiple other political and ecological problems associated with the sector. Thus, discussions of soy production become intertwined with broader debates about agrarian development, industrialization and modernization. Finally, we briefly outline the contributions in this volume, and identify limitations and fruitful directions for further research. 相似文献
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30.
Edson Justino Luiz S. Oliveira Cinthia Freitas 《Forensic Science International Supplement Series》2006,160(2-3):140-147
We describe a procedure for reconstructing documents that have been shredded by hand, a problem that often arises in forensics. The proposed method first applies a polygonal approximation in order to reduce the complexity of the boundaries and then extracts relevant features of the polygon to carry out the local reconstruction. In this way, the overall complexity can be dramatically reduced because few features are used to perform the matching. The ambiguities resulting from the local reconstruction are resolved and the pieces are merged together as we search for a global solution. The preliminary results reported in this paper, which take into account a limited amount of shredded pieces (10–15) demonstrate that feature-matching-based procedure produces interesting results for the problem of document reconstruction. 相似文献