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71.
During criminal investigations involving firearms, the detection of gunshot residues (GSRs) is one of the most important evidences. In the present study, a new method to identify trace evidences of GSRs, deposited around the bullet entrance hole, in different types of fabrics used as targets, is described. The experiments were carried out using a 0.38-inch caliber revolver, and 9-mm and 0.40-inch caliber pistols. Testimonies of 2.25 cm(2) of the fabrics were cut around the bullet entrance and digested with 10% nitric acid. Antimony, barium, and lead were analyzed in the remaining solution using a sector field inductively coupled plasma mass spectrometer. The concentrations of the elements were detected at levels up to few microgram per square centimeter. The use of ternary graphics allowed us to identify specific patterns of distribution for blank samples and the clear distinction between the revolver and pistols used. 相似文献
72.
Błachut D Wojtasiewicz K Krawczyk K Maurin J Szawkało J Czarnocki Z 《Forensic science international》2012,216(1-3):108-120
The synthesis of the designer drug 4-methylthioamphetamine (4-MTA) has been carried out using the well-known Leuckart reaction in four versions. The treatment of 4-methylthiophenylacetone with formamide, mixture of formamide/formic acid, ammonium formate, and mixture of ammonium formate and formic acid followed by acid hydrolysis brought about the formation of 4-MTA contaminated with a number of impurities. The gas chromatography mass-spectrometry (GC-MS) analysis of the reaction mixtures allowed identification of the most prominent impurities, such as diasteromers of N,N-di-[β-(4-methylthiophenyl)isopropyl]amine, N,N-di-[β-(4-methylthiophenyl)isopropyl]methylamine, N,N-di-[β-(4-methylthiophenyl)isopropyl]formamide, the Schiff bases derived from 4-MTA and 4-methylbenzaldehyde (benzaldimine) and 4-methylthiophenylacetone (ketimine) as well as some heterocycles: 4-methyl-5-(4'-methylthiophenyl)pyrimidine, 4-(4'-methylthiobenzyl)pyrimidine, 2,6-dimethyl-3,5-di-(4'-methylthiophenyl)pyridine, 2,4-dimethyl-3,5-di-(4'-methylthiophenyl)pyridine. The correctness of identification was confirmed by independent synthesis of these compounds. Each synthesized reference compound was characterized by means of MS, (1)H and (13)C NMR, and IR methods. The stereochemistry of (RR/SS) diasteromer of N,N-di-[β-(4-methylthiophenyl)isopropyl]amine was confirmed by a crystallographic method. 相似文献
73.
Marek Szydło 《European Law Journal》2012,18(6):793-820
The European legislator, being supported in that regard by the Court of Justice, confers upon national regulatory authorities (NRAs) the exercise of the most important tasks concerned with the regulation of the network‐bound sectors, while at the same time guarantees NRAs a far‐reaching independence in exercising of their discretionary powers and shielding NRAs against other public authorities, including national parliaments. This, in turn, raises many doubts from the perspective of some essential constitutional principles of the Member States, such as, among others, ‘the domain of the law,’ which reserves the regulation of issues sensitive to the citizens as an exclusive parliament's prerogative. It is submitted in this article that national parliaments should play a much more active role in regulating the network‐bound sectors. The main point is to strengthen the protection of fundamental rights of regulated parties and create the real democratic legitimisation of NRAs, while not undermining those regulatory objectives that are already accorded at the EU level. 相似文献
74.
Shells and Bones: A Forensic Medicine Study of the Association of Terrestrial Snail Allopeas micra with Buried Human Remains in Brazil 下载免费PDF全文
Malthus Fonseca Galvão Ph.D. M.D. José Roberto Pujol‐Luz Ph.D. Cristiane Vieira de Assis Pujol‐Luz Ph.D. Cássio Thyone Almeida de Rosa B.Sc. Luiz Ricardo L. Simone Ph.D. M.D. Sônia Nair Báo Ph.D. Karine Brenda Barros‐Cordeiro M.Sc. Larissa Pessoa M.Sc. Giovanna Bissacot D.M.D. 《Journal of forensic sciences》2015,60(5):1369-1372
Little is known regarding the scavenger fauna associated with buried human corpses, particularly in clandestine burials. We report the presence of 20 shells of the terrestrial snail Allopeas micra, within hollow bones of human remains buried for 5 years, during the process of collecting DNA material. The fact that a large number of shells of A. micra had been found in the corpse and in the crime scene supports the assumption that there was no attempt to remove the corpse from the area where the crime occurred. Despite this, our observations cannot be used to estimate the postmortem interval because there is no precise knowledge about the development of this species. This is the first record of a terrestrial snail associated with a human corpse and its role in this forensic medicine case. 相似文献
75.
Kaue Lopes Dos Santos João Sette Whitaker Ferreira 《Bulletin of Latin American research》2023,42(1):131-147
Since the beginning of the twenty-first century, expansion of the formal credit supply in Brazil has promoted the ‘financial inclusion’ of the low-income population, especially through instalment plans offered by large retail chains. This article aims to analyse the impacts of formal credit availability on the consumption of electrical and electronic goods by residents of Jardim Helena, a neighbourhood in São Paulo's periphery. Through the collection and analysis of qualitative and quantitative data, this study reveals how the instalment plan can stimulate consumption among the low-income population, with a significant impact on household budgets, raising the risk of indebtedness. 相似文献
76.
Gusmão L Butler JM Carracedo A Gill P Kayser M Mayr WR Morling N Prinz M Roewer L Tyler-Smith C Schneider PM;DNA Commission of the International Society of Forensic Genetics 《Forensic science international》2006,157(2-3):187-197
The DNA Commission of the International Society of Forensic Genetics (ISFG) regularly publishes guidelines and recommendations concerning the application of DNA polymorphisms to the problems of human identification. A previous recommendation published in 2001 has already addressed Y-chromosome polymorphisms, with particular emphasis on short tandem repeats (STRs). Since then, the use of Y-STRs has become very popular, and a numerous new loci have been introduced. The current recommendations address important aspects to clarify problems regarding the nomenclature, the definition of loci and alleles, population genetics and reporting methods. 相似文献
77.
Frigi S Pereira F Pereira L Yacoubi B Gusmão L Alves C Khodjet el Khil H Cherni L Amorim A El Gaaied A 《Forensic science international》2006,160(1):80-83
The 17 Y-chromosomal short tandem repeats (STRs) included in the AmpFLSTR Yfiler PCR Amplification Kit (AB Applied Biosystems) (DYS19, DYS389I, DYS389II, DYS390, DYS391, DYS392, DYS393, DYS385, DYS437, DYS438, DYS439, DYS448, DYS456, DYS458, DYS635 and GATA H4) were typed in two Berber communities, a small village (Takrouna) and a town (Sejenane), from North Tunisia. As expected, diversity was higher in the town, even when compared with a pool of three small Berber communities, probably due to the combination of different founder effects and genetic drifts operating in the small villages. 相似文献
78.
79.
Mark Carl Rom 《政策研究评论》2005,22(3):369-383
Individual Development Accounts (IDAs) are tax‐protected, matched savings accounts designed to help those with low incomes and few assets buy a home, capitalize a business, or fund higher education. Originally authorized through the Personal Responsibility and Work Opportunity Reconciliation Act (PRWORA), IDAs are designed, implemented, and evaluated through public‐private partnerships. In January 2003 over 500 IDA programs had been created, with more than 10,000 low‐income individuals making contributions. This paper outlines the rationale for IDA as an asset building strategy for the poor, describes the design and operation of IDAs, and provides results of early program evaluations. It concludes by arguing that IDAs are a smart practice that can and should be expanded. 相似文献
80.
Sánchez-Diz P Gusmão L Beleza S Benítez-Páez A Castro A García O Solla LP Geada H Martín P Martínez-Jarreta B de Fátima Pinheiro M Raimondi E Silva de la Fuente SM Vide MC Whittle MR Zarrabeitia MT Carracedo A Amorim A;GEP-ISFG 《Forensic science international》2003,135(2):158-162
A collaborative exercise was carried out by the Spanish and Portuguese ISFG Working Group (GEP-ISFG) in order to evaluate the performance of two Y-chromosome STR PCR tetraplexes, which include the loci DYS461, GATA C4, DYS437 and DYS438 (GEPY I), and DYS460, GATA A10, GATA H4 and DYS439 (GEPY II). The participating laboratories were asked to type three samples for the eight markers, using a specific amplification protocol. In addition, two control samples, with known haplotypes, were provided. The results obtained by the 13 different participating laboratories were identical, except for two laboratories that failed to type correctly the same two samples for GATA C4. By sequence analyses, two different GATA C4 allele structures were found. One control sample (allele 21) and two questioned samples (allele 22, correctly typed by all the laboratories, and allele 25) presented the following repeat structure: (TCTA)4(TGTA)2(TCTA)2(TGTA)2(TCTA)n, but different from the one found for allele 26 in one sample included in this exercise, as well as in the second control sample (allele 23), namely (TCTA)4(TGTA)2(TCTA)2(TGTA)2(TCTA)2(TGTA)2(TCTA)n. The collaborative exercise results proved that both Y-tetraplexes produce good amplification results, with the advantage of being efficiently typed using different separation and detection methodologies. However, since GATA C4 repeat presents a complex structure, with alleles differing in sequence structure, efficient denaturing conditions should be followed in order to avoid typing errors due to sizing problems. 相似文献