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111.
Photodegradation and laser desorption mass spectrometry (LDMS) is a powerful combination of methods capable of characterizing dyes found in pen inks. Rhodamine dyes in pens that contain red ink were analyzed directly from paper (no extraction step is necessary). Inks exposed to incandescent light form photodegradation products (compounds with lower molecular weights than that of the intact dye) and in some instances, photoproducts (compounds with higher molecular weights than that of the intact dye). The degradation products and photoproducts can be detected with LDMS, and the results can be used for dye identification. Advantages include: (1) the instrumental analysis takes less than a minute; (2) sample preparation is minimal; (3) LDMS is a minimally destructive technique; (4) incandescent light sources are inexpensive, safe to use, and readily available; and (5) isomeric dyes can be distinguished. 相似文献
112.
Reports in the literature suggest that diagnostic differences in craniofacial morphology between blacks and whites arise very early in development. These reports, however, have not been consistent regarding which traits are diagnostic and have failed to provide forensic anthropologists with a reliable method of assessment. In an effort to clarify the situation, 13 non-metric craniofacial traits were scored and analyzed statistically in a sample of 70 black and white perinatal specimens obtained from the Smithsonian's fetal osteology collection. Chi-square analysis revealed significant (p<0.05) differences in the distribution of five of the 13 non-metric traits examined. Compared with black perinates, white perinates more frequently possessed a relatively narrow supraoccipital portion of the occipital bone, a prominent anterior nasal spine, "deep" subnasal margins, an elongated vomer, and semi-circular temporal squamae. When these five traits were entered into a stepwise logistic regression, temporal squamous shape, vomer shape and subnasal margin definition were found to be predictive of race (79.1% overall correct classification). An independent sample of 39 black and white perinates was then used to validate the results; overall, 67.5% of the validation sample could be classified correctly. Reasons for the disparity in correct classification rates between the initial and follow-up sample are provided. Results of the present study may be useful for anthropologists who encounter unidentified cranial material from this age range. 相似文献
113.
Paul M. Sniderman Richard A. Brody Jonathan W. Siegel Percy H. Tannenbaum 《Political Behavior》1982,4(2):115-131
This study identifies two forms of evaluative bias toward political objects — positivity and negativity — in addition to the familiar one of partisanship. Bias is measured, predominantly, using open-ended responses to questions on political parties in the NES studies. The incidence of varieties of evaluative orientation toward the parties over time, beginning in 1952, is reported; so also are demographic and cognitive correlates of evaluative bias. Finally, hypotheses on differential assimilation and contrast effects in candidate perception are tested. 相似文献
114.
A case of homicidal strangulation with sodomy is presented. Without the use of a simple routine histologic technique, the diagnosis of sodomy could not have been unequivocally substantiated. 相似文献