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In this study, 13C4-secobarbital was used as an exemplar compound to illustrate the mechanism based on which the effectiveness of a proposed internal standard (IS) could be evaluated. A deuterated analog, 2H5-secobarbital, was also studied in parallel for comparison purposes. Well-established solid-phase extraction and methylation procedures were used prior to the GC/MS measurement step. The contribution of the intensity of an ion designated for the analyte (secobarbital) by the proposed IS, and similarly, the contribution of the intensity of an ion designated for the IS by the analyte--a phenomenon termed "cross-contribution"-were evaluated based on a "direct measurement" procedure in which equimolar amounts of the analyte and the IS were used to generate intensity data. These intensity data were then used as the basis for the calculation of "cross-contribution" (in percentages) of ions designated for the analyte and the IS. Cross-contribution data were compared with the linearity data resulting from two series of standards containing 25 to 9600 ng/mL secobarbital using two sets of quantitation ion pairs--m/z 196/200 and 195/199 with 13C4-secobarbital as the IS and m/z 196/201 and 195/200 with 2HS-secobarbital as the IS. 13C4-secobarbital was found to be much less problematic and thus can serve as a very effective IS. Cross-contribution data alone cannot fully explain the observed differences resulting from the use of these two ISs; further systematic study is needed to provide better understanding of the underlying interference mechanism. 相似文献
204.
As a highly valued ingredient of Chinese medicinal remedies, musk is used as a detoxification agent and for treating fever, inflammation and swelling, and pain. Muscone (3-methylcyclopentadecanone-1), an odoriferous secretion from the ventral glands of male musk deer, is believed to be the active ingredient. A small amount of muscopyridine is also found in the secretion from the ventral glands of male musk deer. Common counterfeit ingredients are musk xylene, musk ambrette, musk ketone, and diphenhydramine. An extraction/GC-MS protocol/data evaluation scheme was developed and applied to study allegedly musk-containing Musk-Tiger Bone Plaster preparations and musk pods (or grains) from Chinese medicine stores and an airport customs. The content of muscone in a specific sample was estimated based on the percentage of the amount recovered from the first extraction. No muscone or counterfeit ingredients were found in all musk pod (or grain) samples from the customs and in the majority of Musk-Tiger Bone Plaster preparations, while muscone (alone or with counterfeit ingredients) was found in most of the musk pod (or grain) collected from Chinese medicine stores. 相似文献
205.
常荔 《江西行政学院学报》2006,8(1):22-24
公务员薪酬制度是社会薪酬制度体系中一个不可分割却又相对特殊的重要组成部分。现行的公务员薪酬制度已稳定运行10余年,在推行公务员制度和保障社会稳定中发挥了应有的作用,但伴随着我国社会、政治和经济环境的巨大变化,现行的公务员薪酬制度在运行和管理中也逐步暴露与外部环境不相适应的结构性障碍。因此,考察公务员整体薪酬现实状况,并揭示其运行和管理中存在的问题,对于我国公务员薪酬制度改革具有重要的现实意义。 相似文献
206.
从利益角度看我国地方政府间竞争 总被引:3,自引:0,他引:3
刘畅 《天水行政学院学报》2006,(1):64-67
通过经济利益、政治利益、文化利益几个方面对我国地方政府间竞争现状的原因进行分析,可以建立利益约束机制、利益分享机制、利益补偿机制来实现协调地方政府间的利益关系,从而促进经济的健康稳定发展。 相似文献
207.
Wong SH Wagner MA Jentzen JM Schur C Bjerke J Gock SB Chang CC 《Journal of forensic sciences》2003,48(6):1406-1415
Pharmacogenomics, applied as an aspect of molecular autopsy, may be used as an adjunct for certifying methadone fatalities. Methadone is metabolized by cytochrome P-450 (CYP) 1A2, 3A4, and 2D6. We hypothesized that methadone toxicity may be partially due to CYP 2D6 *3, *4, and *5 variant alleles, resulting in poor drug metabolism. A retrospective analysis was performed on covariables and risk factors of 21 methadone cases from the Milwaukee County Medical Examiner's Office (1998-2000). PCR genotyping showed: one heterozygous for 2D6*3, two homozygous for 2D6*4, five heterozygous for 2D6*4, and one heterozygous for both 2D6*3 and *4. This limited number of cases showed that the prevalence of poor metabolizer was higher but not significantly different from that of a control group (n = 23) (P > 0.05, Fisher Exact Test). Thus, CYP 2D6 mutations may not yet be directly associated with methadone toxicity. However, pharmacogenomics, complementing other case findings, served as an adjunct in interpreting methadone toxicity of poor and intermediate metabolizers. 相似文献
208.
In this study the structure-induced equilibrium approach for modeling democratic institutions is extended to allow for the added structural features of executive veto and legislative override. A multidimensional model is presented for a budgetary process involving three actors — a legislature, an appropriations committee, and an executive. In order to focus attention on the role of the veto and override possibilities, simplifying assumptions are made with regard to other aspects of the agenda formation process. In particular, the committee has monopoly agenda power, a closed amendment control rule is operative, and perfect-foresight expectations are held by the committee and the executive. Given these assumptions, utility maximization by the several actors generates a budget outcome characterized as a structure-induced equilibrium. The general model is illustrated geometrically with a two-dimensional example, permitting budget outcomes to be analyzed for various combinations of veto rules and override provisions. The analysis demonstrates that budget outcomes are sensitive to alternative specifications of veto rules and override provisions. In the illustration, executive veto power is shown to vary directly with both the permissiveness of the veto rule and the stringency of the override provision. Similar relationships, however, are not found to exist for total budget expenditures. 相似文献
209.
对计算机语言教学方法的探讨 总被引:10,自引:0,他引:10
计算机语言教学在高等教育中具有重要意义。解决计算机语言教学的方法主要有三个方面 ,即调动学生学习的积极性 ;理论联系实际 ;用形象、通俗的语言解释抽象的名词术语、概念及规律。 相似文献
210.
常和平 《中共郑州市委党校学报》2003,3(1):8-10
与时俱进是马克思主义自身的内在要求;与时俱进是马克思主义的鲜明特色;与时俱进是马克思主义创新与发展的正确途径。我们要弘扬马克思主义与时俱进的理论品质,必须以科学的态度对待马克思主义。解放思想、实事求是是引导社会前进的强大力量,是马克思主义的精髓。马克思主义是最讲科学精神、创新精神的,坚持马克思主义,最重要的是坚持马克思主义的科学原理、科学精神和创新精神。 相似文献