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151.
In this study, a new method was developed for the impurity profiling of illicit MDMA tablets. The extraction efficiency, linearity, repeatability and reproducibility of the method were evaluated. Eighty two MDMA tablets coming from presumed unrelated large seizures in 2004 (n >500 tablets) were analyzed by gas chromatography mass spectrometry (GC-MS) in order to assess the discrimination power of the method. The latter was found to be practical, robust, relatively easy to perform, highly discriminative and yielding good chromatography. In addition, some new impurities were detected and identified. Their chemical structures and mass spectra are reported. 相似文献
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153.
Though many years in the making, the UN Human Rights Norms forCorporations only registered on the radars of most states, corporationsand civil society organisations in August 2003 when they beganto move up the ladder of the United Nation's policy-making processes.Since then they have been subject to intense, and sometimesintemperate, debate, scrutiny and controversy. A particularlegal feature of the deliberations has been the focus on theclosely related questions of the legal standing of the Normsin their present format (namely, an imperfect draft, and therefore,of no direct legal force), and what they might become (possiblythoughnot likely soona treaty that speaks to corporations butbinds states). A potent mix of distrust and suspicion, vestedinterests, politics and economics has given rise to a greatdeal of grand-standing and cant concerning these questions andhow they might be answered. In this article, the authors explorethe history of the Norms and the form and content of the debatethat surrounds them, in their attempt to disentangle the legalfrom the rest. That said, the article also focuses on the realpoliticking of the circumstances in which the Norms now findthemselves and it seeks to offer some guidance as to where theNormsor at least their substance, if not their formmightgo from here. 相似文献
154.
C. Haedrich C. Ortmann O.R. Hofmann J. Seilwinder A. Klein 《Forensic Science International Supplement Series》2006,160(2-3):173-177
In a case of suicidal application of electricity differences between the rectal temperature of the body and the suspected time of death were observed.In order to answer the question whether an electric current from hand to hand over >30 min led to a rise in body temperature FEM-based computer simulations and animal experiments were carried out. Both resulted in a warming of the soft parts in the arm without warming the body core. Thus a temperature-based estimation of the time since death can also be used in cases with electricity as the cause of death. Besides, in the animal experiment we found a spontaneous rise in the body core temperature even without application of electricity which may be a reason for the typical temperature plateau after death. 相似文献
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Silvina J. Vilas-Ghiso Diana M. Liverman 《International Environmental Agreements: Politics, Law and Economics》2007,7(2):137-169
More than a decade after NAFTA (North American Free Trade Agreement) entered into force, the environmental effects of agricultural
trade liberalization in Mexico are still controversial, emerging, and not fully understood. This paper contributes to the
literature that aims to explore trends in input use in the agricultural sector in Mexico during the post-NAFTA period among
both commercial/industrial and traditional/rainfed farmers, and examines the influence of the national and multilateral institutional
framework on these outcomes. We decompose the post-NAFTA agricultural production data into scale, technique and composition
effects to estimate the impact that trade liberalization has had on the use of fertilizer and land use, two key agricultural
inputs for which reliable aggregate data is available. We conclude that among commercial farmers patterns of crop type specialization
and significant technological improvements have led to some declines in fertilizer use but they have been offset by growth
in fertilizer use associated with growing agricultural output. Among traditional farmers increased output and specialization
in land-intensive grain crops are contributing to an increase in land under cultivation and technological improvements show
the potential, but not yet not the strength, to counteract these effects. We analyse the environmental institutional framework
and rural development plans, observing that institutional weaknesses have, in several instances, reduced the environmental
benefit of technique and composition effects. We conclude with recommendations about how the Mexican agricultural sector might
reap the environmental benefits of international agricultural trade. 相似文献
160.
Doris Layton MacKenzie David Bierie Ojmarrh Mitchell 《Journal of Experimental Criminology》2007,3(3):221-246
Two hundred thirty four adult male inmates entering prison were randomly assigned to an early release program in either a correctional boot camp or a large, traditional prison in the Maryland state correctional system. Boot camp releasees had marginally lower recidivism compared to those released from the traditional prison. A pre-test, post-test self report survey indicated the boot camp program had little impact on criminogenic characteristics except for a lowering of self control. In contrast, inmates in prison became more antisocial, lower in self control, worse in anger management, and reported more criminal tendencies by the end of their time in prison. Criminogenic attitudes and impulses were significantly associated with recidivism. The impact of the boot camp diminished to non-significance when antisocial attitudes or anger management problems were added to the models predicting recidivism. Implications for jurisdictions considering whether to operate correctional boot camps are discussed. 相似文献