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Gunshot residues originating from six types of pistol ammunition were studied. Six persons who normally have no contact with weapons fired three times, each person from a different pistol. Samples of gunshot residues were collected from the shooters' hands using aluminium stubs with black carbon adhesive tabs and subjected to examinations of their morphology and elemental content by means of a scanning electron microscope with an energy dispersive X-ray spectrometer in an automatic manner. In a comparative study of the samples, only primer residues were taken into account. The frequency of occurrence of particles representing a certain chemical class against the total number of detected particles was expressed as a percentage. Mutual relations between the frequencies of occurrence of the residues of particular chemical content were found to be different for most of the studied ammunition types using a non-statistical approach--and by means of non-parametric statistical methods (R-Spearman and tau-Kendall correlation coefficients), it was possible to differentiate one ammunition type from each of the other ammunition types examined. The performed examinations have revealed some differences in the frequencies of occurrence of certain chemical classes of primer residues, observed for various types of ammunition. These differences could constitute a valuable contribution to group identifications of ammunition made on the basis of physical and chemical examinations of gunshot residues. 相似文献
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Barbara E. Flory Jerry Dunn Marla Berg-Weger Marguerite Milstead 《Family Court Review》2001,39(4):469-482
An exploratory outcome study to investigate the ability of a supervised access and custody exchange center to function as a safe visitation enforcement mechanism of the court was accomplished as part of a larger study investigating child well-being. During a 6-month period of program participation, frequency and consistency of noncustodial parents' access to children dramatically increased and interparental conflict significantly decreased, demonstrating that supervised visitation and custody exchange centers that function in partnership with family court during interim court processes can address the unmet needs of family court and high-conflict domestic disputant as well. 相似文献
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DARA Z. STROLOVITCH 《管理》2008,21(2):306-308
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The stability of tetramine, morphine and meperidine in formalin solution is an important factor for drug analysis in forensic investigation. In this paper, the tissues (liver, kidney, lung and heart) from poisoned rabbits were immersed in 50 ml 10% formalin solutions for 4 months before examination. We compared the levels of tetramine, morphine, meperidine and the main metabolite normeperidine, measured by GC/NPD or GC-MS, in frozen rabbit tissues, formalin-fixed rabbit tissues, and formalin solution. There was a decrease in the levels of tetramine, morphine, meperidine in formalin-preserved tissues compared with the levels of these drugs in the frozen tissues. It is suggested that the formalin-fixed tissues and formalin solution should be analyzed at the same time to assure the accurate results. 相似文献
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