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121.
Maria Cristina Gaudiano Ph.D. Anna Borioni Ph.D. Eleonora Antoniella Ph.D. Luisa Valvo Ph.D. 《Journal of forensic sciences》2016,61(4):1126-1130
A nontargeted approach based on liquid chromatography equipped with a quadrupole time‐of‐flight mass detector (LC‐MS Q‐TOF) joined to nuclear magnetic resonance (NMR) analysis allowed rapid identification and quantification of the anti‐inflammatory drug aceclofenac in illegal Adderall tablets. The largest chromatographic peak had m/z = 354.030 and m/z = 376.012 matching, respectively, the ionic structures (M + H)+ and (M + Na)+ of a molecule M. The accurate mass data generated the molecular formula C16H13Cl2NO4. A screening of the pharmaceutical active substances having that molecular formula together with the MS/MS fragmentation pattern suggested aceclofenac. Aceclofenac structure was unambiguously confirmed by 1H and 13C NMR experiments. The aceclofenac content was 90 mg/tablet (RSD 2%) as detected by quantitative NMR. Information on the identity and content of illegal drugs is required for legal purposes; it supports in evaluating the effective impact on users safety, and it is useful for control laboratories using a targeted approach in their analytical activities. 相似文献
122.
Timothy?J.?LukeEmail author Maria?Hartwig Emily?Joseph Laure?Brimbal Ginny?Chan Evan?Dawson Sarah?Jordan Patricia?Donovan P?r?Anders?Granhag 《Journal of Police and Criminal Psychology》2016,31(4):270-278
The Strategic Use of Evidence (SUE) approach is a framework for planning and executing suspect interviews with the aim of facilitating judgments of truth and deception. US law enforcement officers (N = 59) either received training in the SUE approach or did not. Each officer interviewed a mock suspect (N = 59) who had either committed a simulated security breach or had completed a benign task. The officers who received SUE training interviewed in line with the training: They questioned the suspect systematically, withheld the evidence and critical case information until after questioning, and relied on statement-evidence inconsistency to detect deceit. Consequently, SUE-trained interviewers achieved a higher deception detection accuracy rate (65%) compared to untrained interviewers (43%). 相似文献
123.
Anna Torres Purificación Navarro Fernando Gutiérrez Maria Jesús Tarragona Maria Luisa Imaz Carlos Ascaso Zoe Herreras Manuel Valdés Lluïsa Garcia-Esteve 《Journal of family violence》2016,31(2):137-145
This article describes the development and testing of the psychometric properties of the Partner Violence Entrapment Scale (PVES), an instrument that evaluates the women’s perceived reasons for staying in violent partner relationships. After initial pilot testing, the scale was administered to 213 Spanish women who were victims of intimate partner violence (IPV). An exploratory factor analysis identified six factors: Socio-Economic Problems, Attachment and Fear of Loneliness, Blaming Oneself and Resignation, Impact on Children, Fear of Harm and Worry for the Partner, and Feelings of Confusion. Discriminant validity was established by demonstrating associations between PVES factors and socio-demographic, clinical and abuse variables. The scale appears to be a useful assessment tool for social and clinical settings. Its factor structure, reliability, and validity need to be replicated in other populations and samples. 相似文献
124.
Maria Lipman 《Russian Politics and Law》2016,54(4):341-350
The murder of Boris Nemtsov in February 2015 means that Russian activists know that they may be killed because their public activity is not to the liking of some powerful actor. As the Kremlin has increasingly painted Russia as a country at war, it has created an attitude of emergency state legitimacy in which criticism of the authorities has become a crime. The labeling of some NGOs as foreign agents is part of a continuing trend toward increasing restrictions on civil society. Defense of traditional values and morality has been part of this trend toward increasing repression, which may result in the loss of all protections for activism and free expression. 相似文献
125.
Fiscal Decentralization and Federalism in Latin America 总被引:1,自引:0,他引:1
In contrast to years of centralization when the national governmentdominated the states and municipalities, fiscal decentralizationis now taking place throughout Latin America. This study considersthe reasons for this change. Fiscal decentralization meritsseparate attention because the financial independence of subnationalgovernments ultimately determines their success and power. Competingpolitical and economic explanations are tested on a sample of17 countries between 1985 and 1995. While federalism is a significantpredictor of greater fiscal decentralization, other factorssuch as presidential power, structural adjustment, level ofdevelopment, and country size also determine the level of fiscaldecentralization. 相似文献
126.
Civil society participation in international and European governance is often promoted as a remedy to its much-lamented democratic deficit. We argue in this paper that this claim needs refinement because civil society participation may serve two quite different purposes: it may either enhance the democratic accountability of intergovernmental organisations and regimes, or the epistemic quality of rules and decisions made within them. In comparing the European Union and World Trade Organization (WTO) in the field of biotechnology regulation we find that many participatory procedures officially are geared towards the epistemic quality of regulatory decisions. In practice, however, these procedures provide little space for epistemic deliberation. Nevertheless, they often lead to enhanced transparency and hence improve the accountability of governance. We also find evidence confirming findings from the literature that the different roles assigned to civil society organisations as “watchdogs” and “deliberators” are at times difficult to reconcile. Our conclusion is that we need to acknowledge potential trade-offs between the two democratising functions of civil society participation and should be careful not to exaggerate our demands on civil society organisations. 相似文献
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Charlotte Wagnsson Maria Hellman and Arita Holmberg 《International Political Sociology》2010,4(1):1-14
The globalized security situation characterized by transnational threats and international interventionism in "new wars," connect non traditional local actors and traditional global actors to one another in unprecedented ways. We argue that children in particular need to be highlighted because they are highly pertinent to the globalized security situation, yet they make up one of the few agents that have remained non-politicized in the eyes of the scholarly community. The article suggests a framework of analysis that can generate analyses on security of traditional as well as non-traditional agents. Placing non-traditional groups in the center of attention serves to mirror the complexities of the current security situation better. 相似文献
130.
The adoption of the Treaty of Lisbon and the granting to the Charter of Fundamental Rights of the same legal force as the Treaty has lent a new impulse to the consideration of fundamental human rights by the European Union (EU). The question remains, however, as to how this legal discourse, centred upon human rights, is actually shaping the EU regulatory framework in specific policy domains. The aim of this paper is to critically appraise the ways that the fundamental rights of security, privacy and freedom guaranteed by the Charter are being construed in the context of EU law and policy on biometrics, an ethically and morally sensitive security technology whose development and use are being actively promoted by the EU. We conclude that the interpretation of the pertinent rights, as well as their balancing, owes a great deal to the goals of EU policies for research and development, and under the auspices of Freedom, Security and Justice, shaped largely by political and economic considerations. These considerations then tend to prevail over ethically or morally-based legal claims. 相似文献