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排序方式: 共有310条查询结果,搜索用时 46 毫秒
51.
Laser detection of latent fingerprints on a white paper has been performed, previously. Ultraviolet fluorescence from various kinds of printer toner and ink used for home printers were measured to study fluorescence imaging of fingerprints on a color-printed white paper. The experimental system consisted of a nanosecond pulsed tunable laser and a cooled CCD camera. Excitation wavelengths are 230 and 280 nm. Fourteen printers consisting of three color laser printers, three color inkjet printers, five monochrome laser printers, two monochrome copy machines, and a color copy machine were tested. Toner and ink of most printers exhibited fluorescence in the region from 360 to 550 nm. In most cases, clear fluorescence images were obtained by time-resolved imaging with a band-pass filter and 280-nm excitation. However for toners from laser color printers that showed strong fluorescence, better results were obtained with 230-nm excitation. Latent fingerprints on a photograph page and a black-character page of a newspaper were also imaged. 相似文献
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Sugawara S 《Journal of forensic sciences》2007,52(4):974-977
In this study, a new nondestructive technique for passport examination is proposed. In this technique, linearly polarized light is used to measure Fourier transform infrared (FT-IR) reflectance spectra of films on the biographical data page. Thirty genuine and thirty-five counterfeit Japanese passports and five marketed films pasted on name cards were examined. The measured spectra were analyzed as follows. The absorption spectra were obtained by the Kramers-Kronig transformations of reflectance spectra. The peak ratios were then calculated from the absorption spectra by adding the peak areas at 1126 and 1263 cm(-1) and dividing the result by the peak area at 1727 cm(-1). When nonpolarized light was used, the samples could not be distinguished by comparing the peak ratios. However, when polarized light was used, they were successfully distinguished by the comparison. Therefore, polarized light is useful for the forensic discrimination of passport films by the measurement of FT-IR spectra. 相似文献
55.
Suspects in shooting investigations in Chicago are routinely transported in department vehicles and detained in department facilities prior to gunshot residue (GSR) evidence collection. The GSR test results are used to associate the suspect with primary exposure to GSR. The potential for these vehicles and facilities being sources of secondary GSR contamination needed to be determined. A total of 201 samples were collected from randomly selected vehicles and detention facilities. The sampling collected trace materials from surfaces that suspects' hands may contact during the arrest process. These samples were examined for the presence of GSR particles using scanning electron microscopy. Upon completion of the automated analysis, those particles that met an initial GSR screening criterion were relocated and reanalyzed. The locations where GSR particles were recovered allowed us to make recommendations to the Chicago Police Department with regard to transporting and detaining these suspects. The low number of GSR particles recovered suggests that the potential for secondary contamination, although present, is relatively low. 相似文献
56.
Robert G. Weston M.Sc. 《Journal of forensic sciences》2010,55(4):1068-1075
Abstract: The analysis of mixtures of “crystal meth” (usually comprised of methyl sulfone [MS] and methamphetamine [MA]) by gas chromatography‐mass spectrometry (GCMS) is routine in many forensic drug laboratories. The utilization of Raman spectroscopy for the identification of such mixtures quickly and without the need for a separation technique is discussed. Samples were dissolved in water and Raman spectra of the resulting aqueous solutions were collected. By comparing these spectra to spectra of methylsulfone and MA mixtures of known composition, an indication of the composition of the sample can be obtained in only a few minutes. This spectral comparison also can be used as a semi‐quantitative analysis of MA concentrations in such exhibits. 相似文献
57.
Kelly M. Brinsko M.S. 《Journal of forensic sciences》2010,55(4):915-923
Abstract: Fibers that are termed “eco‐friendly” or “biodegradable” by manufacturers are increasingly being used in textile products such as apparel and carpeting to appeal to the ever more environmentally aware public. As such, these modern fibers are expected to begin showing up more often in forensic casework, and it is important that the forensic examiner recognize them. This study employed polarized light microscopy (PLM) and Fourier transform infrared (FTIR) microspectroscopy to characterize selected fibers of azlon, polylactic acid (PLA), cellulose composites of alginate or chitin, and bamboo (viscose rayon). Fiber cross‐sections, refractive indices, melting points, solubilities, and FTIR measurements were conducted. Results indicate that the azlons and PLA fibers are easily distinguishable from other textile fibers by their optical and chemical properties. The cellulose composites show only small differences in comparison with other cellulose‐based fibers, while bamboo viscose rayon is indistinguishable from normal viscose rayon. 相似文献
58.
Norimitsu Akiba Ph.D. Kenro Kuroki Ph.D. Kenji Kurosawa Ph.D. Ken'ichi Tsuchiya Ph.D. 《Journal of forensic sciences》2018,63(2):556-562
Detection of aged fingerprints is difficult because they can degrade over time with exposure to light, moisture, and temperature. In this study, aging fingerprints were visualized by time‐resolved spectroscopy with an ultraviolet‐pulsed laser. Fingerprints were prepared on glass slides and paper and then stored under three lighting conditions and two humidity conditions for up to a year. The fluorescence intensities of the fingerprints decreased with time. Samples were stored in the dark degraded less than in sunlight or under a fluorescent lamp. Samples were stored under low humidity degraded less than under moderate humidity. As the storage period increased, a fluorescence emission peak appeared that was at a longer wavelength than the peak visible in earlier spectra. This peak was used for visualization of an aged fingerprint over time. An image of the fingerprint was not initially visible, but an image appeared as the time since deposition of the fingerprint increased. 相似文献
59.
Controversial Suicide Case Using a Submachine Gun with a Sound Suppressor—The Need of Team Work of Forensic Chemistry and Firearm Examiners
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Zuzanna Brożek‐Mucha Ph.D. Krzysztof Zdeb M.Sc. Eng. 《Journal of forensic sciences》2018,63(3):921-929
Evidence materials in a presumed suicide case were studied by a firearm examiner and a forensic chemist. The victim's body with double gunshot wounding in his forehead, a machine gun in the sustained fire mode with a silencer, and four cartridge cases were found. Examinations of the evidence, the case file studies, and experiments dedicated to the case were carried out. Relationships between the placement of cartridge cases and the gun were established using a fast camera. The distributions of gunshot residues on the evidence materials and within the comparative gunshot patterns were studied by means of optical and electron microscopy, X‐ray microanalysis, and infrared spectroscopy. The shooting distance was assessed to be 30 cm or more, whereas the greatest distance that could have been achieved by the victim himself was about 11–13 cm. The obtained results supported the version of homicide rather than suicide. 相似文献
60.
Diana M. Wright Ph.D. Maureen J. Bradley Ph.D. Andria Hobbs Mehltretter M.S. 《Journal of forensic sciences》2013,58(2):358-364
Comparative analyses of 50 single‐layer white architectural paints were conducted to determine the discrimination power using standard techniques and to provide a basis for assessing significance when paints with limited features are not discriminated. Utilizing Fourier transform infrared spectroscopy (FTIR), 68 undifferentiated pairs resulted, yielding a discrimination of 94.45%. Adding stereomicroscopy, scanning electron microscopy (SEM) with energy dispersive spectroscopy (EDS) and backscatter electron (BSE) imaging, and pyrolysis‐gas chromatography/mass spectrometry (Py‐GC/MS), the overall discrimination was 99.35%. The study included blind verification replicates, which resulted in the only pairs without indications of physical or chemical differences. The remaining groups of undifferentiated samples contained subtle differences by at least one technique, but were considered undifferentiated for the discrimination power evaluations. This study demonstrates a high degree of discrimination of single‐layer white architectural paints using methods of analysis often encountered in forensic science laboratories. 相似文献