尿液、血液中γ-羟丁酸的气质联用法分析

目的为尿液、血液中γ-羟丁酸(gamma-hydroxybutyricacid,GHB),γ-羟丁酸内酯(gamma-butyrolactone,GBL)和1,4-丁二醇(1,4-butanediol,1,4-BD)的鉴定提供方法和依据。方法100μl尿液或血液以GHBd6为内标,经乙酸乙酯提取、BSTFA衍生化后,用GC／MS法分析。结果测尿液中内源性GHB的线性范围是20-800ng／ml,R2=0.9995,最低检出限为10ng／ml(S／N≥3);测尿液、血液中外源性GHB的线性范围为5-60μg／ml,R2分别为0.9999和0.9928。相对回收率为99％-104％。以所建方法测定了健康志愿者尿液中内源性GHB含量,并考察了健康受试者外源性GHB的代谢情况。结论所建方法准确、便捷、省时、选择性好,适用于法医毒物学鉴定。     

GC／MS检测尿中4种苯氧羧酸类除草剂

目的建立尿中2，4-D、2，4-DP、MCPA、MCPP等4种苯氧羧酸类除草剂的分析方法；方法液液提取分离，乙醚为提取液，DCPA为内标，硫酸正丁醇酯化衍生化，气质联用分析法分析；结果尿中4种除草剂添加样品的相对回收率在80％以上，检测限都在5ng／ml以下，对中毒兔尿样进行了分析；结论对实际发生的中毒案件分析有足够的灵敏度。     

证言真实性的审查与判断——陈述有效性评估技术

在证言研究中有一著名的理论假设:即来自于真实经历的证言与经他人教唆或自己幻想产生的证言是有区别的。现代的法庭科学与司法心理学也证实了"亲身经历过的事件记忆与想象记忆有着质的差异"。建立在上述差异基础上所形成的陈述有效性评估技术,专门用于检测言词的准确性,现已经在一些西方国家得以运用,在个别国家还甚至被运用于刑事领域。     

心理测试技术中情绪机制的应用

心理测试技术是一项多学科综合应用的产物,但心理学是其最重要的理论根基和发展动力。个体情绪机制是心理测试技术存在和应用的一个重要的心理学原理。在实际应用中,还必须结合犯罪嫌疑人情绪机制的特点,分析其在测前谈话中的调动作用,在正式测试中的聚焦作用和在测后谈话中的突破作用。     

Development and validation of the Cozart DDS oral fluid collection device

The testing of oral fluid for drugs of abuse has increased significantly over recent years and is now commonplace in drug rehabilitation clinics, the workplace, prisons and custody suites. The global problem of identifying drugged drivers has also led to an increase in oral fluid testing at the roadside. The main requirements for the implementation of roadside drug testing are a rapid sample collection time, collection of a known sample volume and recovery of drugs from the collection device. We report here the development of the Cozart^® DDS oral fluid collector, an oral fluid collector that combines rapid and adequate sample collection with satisfactory drug recovery. Oral fluid was collected from drug users (n = 134) and drug-free individuals (n = 137), using the Cozart^® DDS oral fluid collector. The mean time for the completion of collection (full coloration of the sample presence indicator) was 34 s for drug-free individuals and 44 s for drug users. The average volume collected was 0.34 mL (n = 271). No chemical stimulant (to induce salivation) was used to achieve the collection times observed in either the drug-free or the drug-taking sample populations. Drugs were extracted from the collector using the Cozart^® DDS buffer and drug recovery was determined by Cozart^® enzyme immunoassays. The recovery studies showed that for amphetamine, Δ⁹THC, cocaine, methadone, methamphetamine, morphine and temazepam over 90% of the drug in the sample was eluted from the collector. The Cozart^® DDS oral fluid collector provides a reliable mechanism for the collection of oral fluid at the roadside that achieves the rapid collection times required.     

The Error in “Error Rate”: Why Error Rates Are So Needed,Yet So Elusive

Establishing error rates is crucial for knowing how well one is performing, determining whether improvement is needed, measuring whether interventions are effective, as well as for providing transparency. However, the flurry of activities in establishing error rates for the forensic sciences has largely overlooked some fundamental issues that make error rates a problematic construct and limit the ability to obtain a meaningful error rate. These include knowing the ground truth, establishing appropriate databases, determining what counts as an error, characterizing what is an acceptable error rate, ecological validity, and transparency within the adversarial legal system. Without addressing these practical and theoretical challenges, the very notion of a meaningful error rate is limited.     

Distributed Generation of Electricity: The Role of Academic Research and Advice in California’s “Clean DG” Policy Network

Deregulation and the combined threats of energy crises and global warming concern nations around the world, yet these issues continue to be addressed more directly by domestic regulatory systems than by international institutions. The present analyses of the integration of distributed sources of power generation (DG) into California’s electric utility system suggests that domestic environmental dilemmas with international repercussions provide an obvious entrée for global environmental policy specialists into the practice of environmental policy-making and law. Here I review current scholarship on policy networks that illuminates the contributions that technical and policy experts can make to such networks surrounding environmental issues. I then introduce the key members of California’s “clean DG” policy network that emphasizes the role of academic experts in this influential political system, and discuss how my own research has impacted the development of the state’s DG policy. I conclude that scholars are well positioned to observe and engage domestic and international environmental policy networks, and thereby also to influence environmental politics and law.     

司法心理测试技术应用研究成果综述

广东省公安司法管理干部学院侦查系参与了国家“九五”科技攻关项目——司法心理测试技术、设备及应用研究,承担应用研究子专题任务。课题组采用实验研究和现场实案测试研究相结合的方法,完成了合同规定的研究任务,取得了重要成果。其成果主要内容如下:测谎技术用于区分犯罪施行者、知情者和无辜者研究;反测谎识别及其对策研究;测谎技术在刑事案件侦查中的应用研究;测谎基础理论的探讨;测谎技术应用情况;本课题研究对测谎技术的创新点。     

Diagnostic Value of PSA and AP Tests for the Detection of Spermatozoa in Postmortem Swabs from the Genital and Anal Region in Males

The aim of this study was to clarify whether positive results for prostate‐specific antigen (PSA) and acid phosphatase (AP) occur in postmortem swabs from the genito‐anal region in males (n = 80; 4 regions) and females (n = 20; 3 regions) and to calculate the positive predictive value (PPV) concerning the presence of spermatozoa. In male subjects, the highest incidence of positive test results was found in urethral swabs (PSA 76%, AP 71%) and the lowest frequencies appeared in perianal and rectal swabs (15–20%). Microscopic evaluation for spermatozoa was positive between 39% in urethral swabs and 1% in rectal swabs. PPV regarding positive identification of spermatozoa was 33.3% for PSA and 31.5% for AP. The combination of both tests yielded a PPV of 38.2%. In female cases, no spermatozoa were identified, and one case was PSA‐ and AP‐positive in perianal swabs. Our findings indicate that PSA and AP tests are of limited value for the postmortem detection of spermatozoa in male subjects.