“切开法”快速鉴定朱墨时序

朱墨时序是指印文与字迹形成的先后顺序。"朱"代表印文,"墨"指与印文形成交叠的字迹笔画。用"切开法"进行光敏印油、印泥印文和喷墨打印字迹、激光打印字迹、复印字迹的朱墨时序鉴定实验,取得了令人满意的效果。实验证明,"切开法",所需器材简单,操作简便,准确率高,对鉴定人从业经验也没有很高要求,非常适合基层一线单位使用。     

利用激光、光敏印章机伪造印章印文的鉴定

利用激光刻章机雕刻、光敏印章机制印伪造印章印文是近年来出现的一种新的、仿真程度较高的伪造印章印文的方法。鉴定实践表明,这类伪造印章印文趋于专业化、技术化,且伪造的印章印文与真实印章印文的相似度较高。依据传统的鉴定依据和方法难以鉴别真伪,因此从该类伪造方法对其特点和鉴定依据、方法要点进行研究,尤其是对伪造形成方式及特点的研究,有助于科学的鉴定其真伪。     

Age determination of ballpoint pen ink by thermal desorption and gas chromatography-mass spectrometry

Two main approaches can be used for determining the age of an ink: indirect dating and direct dating. Indirect dating is based on the chemical analysis of an ink followed by comparison with known samples in a reference collection. The collection should contain information about the inks including the market introduction dates. This approach may allow for an anachronism to be detected. The second concept is based on measuring ink components that change with age. The analysis of solvents in ballpoint inks may be a useful parameter for determining the age of ink on paper. In a previous study, the authors demonstrated that thermal desorption of ink directly from paper, followed by chemical analysis using gas chromatography-mass spectrometry (GC-MS), is a promising procedure for characterizing ink-binder resins and solvents. Preliminary tests showed that monitoring the evaporation of ink solvent from ink on paper is not a suitable method for ink dating. Thermal analysis of ink on paper in two steps revealed that fresh ink releases a relative amount of solvent at a certain low temperature in a defined period of time, which decreases as the ink ages. As a consequence, this relative amount of solvent released at a certain low temperature, and its decrease with time, can be used to estimate ink age. This age-dependent parameter was studied in 85 different inks ranging in age from 1 week to 1.5 years. It was found that some inks showed a significant decrease of this parameter up to an age of several months, and that the aging process can be monitored within this period. For other inks, however, the age-dependent parameter decreases relatively fast, e.g., within a few days, to a constant level, which can be too fast for casework. Based on these results, a general procedure for assessing the age of ballpoint pen inks on paper was developed.     

Identification of colorants in pigmented pen inks by laser desorption mass spectrometry

Pigments are rapidly replacing dyes as colorants in pen and printer inks, due to their superior colors and stability. Unfortunately, tools commonly used in questioned document examination for analyzing pen inks, such as TLC, cannot be used for the analysis of insoluble pigments on paper. Laser desorption mass spectrometry is demonstrated here as a tool for analyzing pigment-based pen inks. A pulsed nitrogen laser can be focused onto a pen stroke from a pigmented ink pen on paper, and positive and negative ions representative of the pigment can be generated for subsequent mass spectrometric analysis. Targeted pens for this work were a set of Uni-ball 207 pigmented ink pens containing blue, light blue, orange, green, violet, red, pink, and black inks. Copper phthalocyanine was identified as the pigment used to make both blue inks. A mixture of halogenated copper phthalocyanines were identified in the green ink. Unexpectedly, the pink ink was found to contain a red pigment, Pigment Red 12, treated with a mixture of water-soluble dyes. Each sample yielded ions representative of the pigments present.     

Identification and dating of the fountain pen ink entries on documents by ion-pairing high-performance liquid chromatography

A novel approach for the identification and dating of the fountain pen ink entries on paper has been established by ion-pairing high-performance liquid chromatography (IP-HPLC). Twelve black and six red fountain inks have been collected, and their ink entries have been prepared by drawing lines on paper. The chromatographic conditions for separation of their dye components after extraction with solvents were optimized. Under the optimized conditions, the 18 fountain pen inks were differentiated individually by comparing the number of detectable main or minor dye components, and the relative peak intensities of each component. The ink entries were artificially and naturally aged, and the analysis results showed that the ink dye components were significantly decomposed when exposed to UV or fluorescent light compare to those of inks stored under natural condition. The changes of the relative peak height for the dye components were linearly related to the aging time, especially under natural aging conditions. The degradation characteristics of the dye components under different aging conditions provide scientific evidences for dating of the suspicious fountain pen ink entries on document.     

书写时间确定技术的国内现状与发展

综述了书写时间确定技术在国内的现状及最新发展,主要从三方面进行了介绍:水溶性书写时间确定技术;圆珠笔油墨书写时间确定技术;间接确定文件的书写时间方法。     

Use of lycode powders for the examination of documents partially written with erasable ball point pen inks

It was discovered by change that lycode powders adhere to erasable ball point pen ink strokes. A study of this phenomenon was carried out to determine what type of inks reacts physically with lycode powders. A further evaluation was made to learn if this effect continued after the erasable ink became indelible. It was also found that obliterated erasable ball point pen ink can be read by applying lycode powders and that the powders react in a similar way with typewriting from a conventional inked typewriter ribbon. Treatment in this case is completely non-destructive since the lycode powder can be wiped off the paper surface.     

不同纸张上浓重红色印泥手印减薄的技术研究

目的建立有效的显现纸张上浓重的印泥手印方法。方法对普通材料纸和打印纸上的浓重红色印泥手印，通过指纹胶带提取转印、氧化漂白减薄、有机溶剂溶解减薄3种技术方法的减薄效果以及它们在减薄过程中的优缺点进行比较，得出适合于各种减薄技术的最佳试剂。结果本研究发现3种方法均可以有效地使浓重红色印泥手印清晰化，进而达到有效显现纸张上浓重的印泥手印的目的。     

几种墨水材料的检验

墨水是书写文字的常用材料,其种类很多。根据化学成分及用途的不同,可分为蓝黑墨水、染料墨水、碳素墨水及其他墨水。在侦查工作中时有遇到用该种书写材料涂抹掩盖等情况,故此,墨水材料的检验鉴定,在侦破此类案件中起着十分重要的作用。     

the Westin Beijing Financial Street Welcomes New Italian Chef domenico Cicchetti

正Domenico Cicchetti,the new Head Chef of Prego Italian Restaurant at The Westin Beijing Financial Street,has massive culinary experience in international five-star hotels,having served successively in the Grand Hyatt Sao Paulo,Brazil,and one of the