A comparison of the use of visible microspectrometry and high performance thin layer chromatography for the discrimination of aqueous inks used in porous tip and roller ball pens

Ink lines made by porous tip and roller ball pens have been examined by high performance thin layer chromatography (HPTLC) and by transmission microspectrophotometry (VM) in the visible region. Better discrimination between apparently similar coloured inks was obtained with HPTLC but VM has value as an additional technique for ink examination.     

见义勇为高风险的化解

由于见义勇为不是公民的法定义务,过多地从道德上谴责"见义"而不敢"勇为"的人并不能收到良好的效果。有人用《好撒玛利亚人法》作为见死不救入罪的根据,其实是一种误读。道德的高尚性可以用"真、善、美"三个字来概括,"真、善、美"这三个字所表达的内涵是一致的,为善求美也要实事求是、量力而行。倡导在见义勇为时防范、降低风险,保护自身安全,无论对社会、对见义勇为者都具有重要意义。政府应当学会多层次聚焦见义勇为的正能量,见义勇为者也应当尽可能地减少风险。     

HPLC测定复方丹皮酚凝胶中丹皮酚含量

目的:建立复方丹皮酚凝胶中丹皮酚的含量测定方法.方法:采用高效液相色谱法,色谱柱为SHIMADZU VP-ODS(4.6 mm×150 mm, μm),流动相为甲醇-水(50∶50),检测波长为274 nm.结果:丹皮酚进样量为0.05～0.30 μg时呈良好的线性关系(r =0.999 8).平均回收率为100%,SD为0.87%(n =5).结论:PLC法可用于复方丹皮酚凝胶的质量控制.     

日本知识产权高等法院研究

知识产权高等法院的设立是日本“知识产权立国”政策最大的亮点,其主要目的是建立技术类知识产权案件二审的专门法院,并设立了大合议、法院调查员和专门委员制度。由于特许厅在专利的数量控制上占优势,故特许厅的审判前置在确保专门性这一点上仍具有独立的价值。另一方面,知识产权高等法院为实现多元集中化进行了各种尝试,然而该尝试时常受到大合议的干扰,因此需要避免大合议过早干预,同时须处理好知识产权高等法院与最高法院的关系,形成良好的运行机制。     

益化清解方对2型糖尿病大鼠炎性分子网络的影响

[HT5K]目的:观察益化清解方对2型糖尿病（T2DM）大鼠炎性分子网络调控的影响。方法:复制T2DM大鼠模型,治疗组用益化清解方中药灌胃,并与模型组、二甲双胍组及正常组作对照。分别在给药前和给药第15,30天检测T2DM大鼠的肿瘤坏死因子 α（TNF α）、白介素6(IL 6）、高敏C 反应蛋白（hsCRP）、脂联素(Adiponectin,Adp)、瘦素(leptin）水平,探讨其变化与空腹血糖（FBG）、血清胰岛素（FINS）及胰岛素敏感性指数（ISI）的关系;并检测各组大鼠脂肪组织脂联素及骨骼肌组织脂联素受体R1 Mrna表达水平,探讨Adp、Adp受体与这些因素之间的关系。结果:益化清解方能显著降低T2DM大鼠血糖、血脂、C反应蛋白等水平,并提高胰岛素敏感性,改善糖尿病大鼠的脂肪组织Adp Mrna表达水平。结论:益化清解方对糖、脂双调节的作用可能是通过增加胰岛素敏感性而实现的,其与改善糖尿病大鼠的脂肪组织Adp Mrna表达相关.     

审理存单纠纷案件若干问题探讨

最高人民法院公布的《关于审理存单纠纷案件的若干规定》司法解释施行八年来,全国法院依据该司法解释审结了大量的存单纠纷案件,取得了丰硕的成果,但是在适用该司法解释时各地法院的认识却不尽相同,特别是在存款的所有权归属、存单的法律特征、以存单为表现形式的借贷纠纷案件的认定、公款私存问题等方面的认识仍存在分歧,本文将对上述问题进行分析。     

The High Representative and directoires in European foreign policy: the case of the nuclear negotiations with Iran

ABSTRACT

The negotiations with Iran about its nuclear programme have seen the most protracted involvement of the High Representatives of the European Union in a high-profile policy case. This article traces the evolution of the High Representatives’ participation in the negotiations, from the first contacts with the E3 (Germany, France and the United Kingdom) in 2003 to the adoption of the Joint Comprehensive Plan of Action in 2015. It focuses on the institutional role the High Representatives played in relation with the directoires leading the talks with Iran – first the E3 and, since 2006, E3/EU. In this context, it examines the personal and organisational factors that affected the influence each of the three High Representatives (Javier Solana, Catherine Ashton and Federica Mogherini) had in regard to the directoires. The analysis distinguishes specifically between the phases before and after the 2009 Lisbon Treaty. The article shows how similar personal qualities of the three High Representatives in terms of problem-solving and trust-building gave them political capital that enabled them to adopt a fairly constant role as bridge-builders within the directoires and between the directoires and other actors. The reforms of the Lisbon Treaty had only a minor impact.     

Acknowledging the Suffering Caused by State-Mandated Sexual Violence and Crimes: An Assessment of the Iraqi High Tribunal

The Iraqi High Tribunal (IHT), as a mechanism of transitional justice, took upon it a pioneering role within the Middle Eastern Region by prosecuting and convicting several high-ranking members of the former suppressive regime in Iraq. As part of this work, the IHT confronted the widespread impunity for and disregard of gender-based crimes, such as rape and other sexual violence, and took steps towards reforming the sector through its progressive statute and the specific acknowledgment of gender crimes within its judgments. It will be the aim of the following article to extend academic writings on Iraq, the IHT and gender, by providing insights into how the tribunal dealt with the issues of rape and sexual violence, the surrounding circumstances and how successful the IHT's recognition of these crimes proved for transitional justice in Iraq.     

Catching Them Before Too Much Damage is Done: Early Intervention with Resistance‐Refusal Dynamics

Children often need help before their parents are ready to stop fighting. Children at the center of high‐conflict disputes, particularly those who resist contact with a parent, face extraordinary risks of maladjustment. Years of investigation and litigation may precede any meaningful attempt at intervention, based on the questionable belief that all elements of causality (or blame) must be established before any effective treatment can occur. Children's functioning may continue to deteriorate during this time, undermining their future adjustment and reducing the chance of successful intervention later. We illustrate the application of the coping‐focused, multisystemic Child Centered Conjoint Therapy model to assisting these families. Methods to assist children without compromising external investigations are discussed.     

Co‐parenting in a Highly Conflicted Separation/Divorce: Learning about Parents and their Experiences of Parenting Coordination,Legal, and Mental Health Interventions

Sixty high‐conflict separated/divorced co‐parents completed surveys investigating characteristics and dynamics (narcissism, empathy, conflict) that were examined in relation to co‐parenting style and parents' experiences of parenting coordination, legal, and mental health interventions. Study findings for this sample did not support common notions found in the literatures on parenting coordination and high‐conflict divorce that suggest these parents are often narcissistic or low in empathy. Findings pertaining to all high‐conflict participant experiences revealed the presence of common elements across aspects of practitioners and interventions with which they were both satisfied and dissatisfied.