论大数据技术对公安工作的影响

大数据具有的4V特性决定了大数据技术将从多个角度和层面丰富侦查方式,提高了各类案件的侦破效率;以高科技预防高科技犯罪,做到打击迅速、减少损失,还百姓以现实的安全感;整合多种资源,引导社会运转,预见行为规律,构建令百姓满意的和谐治安环境;让公安工作始终开展的公正透明,百姓享有现实与虚拟环境里的平等权利;提供高效的管理手段和模式,不断推动社会管理的创新。全面认识大数据技术对公安工作的影响,有利于推动公安工作上台阶,不断实现新的突破。     

酮洛芬注射液在乳牛体内的残留消除研究

为建立牛乳中酮洛芬的液相色谱-串联质谱(LC-MS/MS)检测方法,牛乳样品经甲醇提取,C18色谱柱分离,采用正离子模式,多反应监测,内标法定量。结果表明,牛乳中酮洛芬的检出限为1μg/kg,定量限为5μg/kg,在5~200μg/kg范围内线性关系良好,相关系数大于0.99。在25~100μg/kg添加水平的回收率为93.3%~107.5%,批内、批间相对标准偏差分别为1.72%~5.46%、1.13%~7.04%。该方法高效、灵敏、准确,可作为牛乳中酮洛芬的检测方法。选用20头健康的泌乳期荷斯坦乳牛,高产、低产各10头,以3 mg/kg剂量肌内注射给药,每天1次,连用3 d,分别于每次给药后第2、15小时采集乳样。每次给药后2 h牛乳中可检出酮洛芬,最高质量分数为(38.43±3.90)μg/kg,停药后15 h均未检出。所有时间点牛乳中酮洛芬质量分数的实测结果均低于加拿大规定的最高残留限量50μg/kg,建议弃乳期为0 d。     

对宗教"五性"的再认识

宗教“五性”是马克思主义宗教观与我国社会宗教实际相结合的产物 ,是马克思主义宗教理论在新的历史条件下的坚持和发展 ,是完善和正确执行党的宗教政策的基本点。我国正处于社会转型时期 ,对宗教“五性”的再认识 ,是我们进一步深化对国情的再认识。     

“众创时代”共青团院校创业教育的发展

在大众创业、万众创新的时代,共青团院校应该通过发挥团青引领优势、创新优势、桥梁优势、覆盖优势等,大力发展创业教育。通过培养大学生、青年、团员的创新创业能力,为社会经济繁荣和社会治理发展做出贡献。当然,共青团院校创业教育要更好地发挥其独特作用,还应该在争取党和政府制定激励共青团院校创业教育的政策、探索"全员创业教育"的新型机制、师生树立多元化创业教育的新观念、将创新创业贯穿人才培养的全过程、与青年企业及机构建立"无缝对接"以及加大创业教育的国际交流与合作等方面做出努力。     

再论公安工作与群众路线

坚持和贯彻群众路线是公安机关的优良传统和特色。在新世纪新形势下,公安机关必须继承和发展群众路线,解放思想,与时俱进,不断创新群众路线,从而更加有效地发挥职能作用。     

转型期劳工群体性事件的客观成因

当前,我国正处在一个社会转型期,这一时期的劳工群体性事件呈急剧增加态势。此类事件的频繁爆发有其深刻的客观原因,主要表现在经济、政治和社会三个方面。     

提升中俄经贸关系需要媒体助阵

从新闻传播的真实性与公正性原则出发,探讨媒体在中俄战略伙伴关系中发挥的三种作用:“尊重事实避免虚假新闻”、“摒弃炒作负面新闻”和“引导沟通充当经贸桥梁”。目的在于从大众传媒领域找到推进中俄战略伙伴关系的新动力。     

The Effect of Temperature and Exposure Time on Stability of Cholesterol and Squalene in Latent Fingermarks Deposited on PVDF Membrane

Cholesterol and squalene are fatty materials of latent fingermarks that can be utilized for dating methodologies and visualization techniques. Previous studies have suggested these compounds undergo degradation in fingermarks as a function of time (days) and light at ambient temperature. However, studies assessing how their composition changes at low and high temperatures over short periods of time (hours) have not been published previously. Here, we performed quantitative analysis of cholesterol and squalene in natural fingermark residue using PVDF membrane, after exposure to a range of temperatures (−20 to 100°C) for 4 and 8 h. We found that levels of both fatty materials remained constant at −20 to 60°C, but both showed significant reduction at 100°C, over short exposure times. These results indicate that cholesterol and squalene are detectable at −20 to 60°C, whereas at 100°C or higher, both are lost due to rapid thermal degradation.     

Sample Mining and Data Mining: Combined Real-Time and Retrospective Approaches for the Identification of Emerging Novel Psychoactive Substances

Novel psychoactive substances (NPS) are synthetic drugs that pose serious public health and safety concerns. A multitude of NPS have been identified in the United States, often implicated in forensic investigations. The most common and effective manner for identifying NPS is by use of mass spectrometry and the true utility lies within nontargeted acquisition techniques. During this study, a liquid chromatography quadrupole time-of-flight mass spectrometry (LC-QTOF-MS) assay was developed, validated, and implemented for forensic toxicology testing. A SCIEX TripleTOF™ 5600 + with SWATH^® acquisition was used. Resulting data were compared against an extensive library database containing more than 800 compounds. The LC-QTOF-MS assay was applied to the reanalysis of biological sample extracts to discover emergent NPS. More than 3,000 sample extracts were analyzed, and more than 20 emerging NPS were detected for the first time. Among these were isopropyl-U-47700, 3,4-methylenedioxy-U-47700, fluorofuranylfentanyl, N-methyl norfentanyl, 2F-deschloroketamine, 3,4-methylenedioxy-alpha-PHP, eutylone, and N-ethyl hexedrone.     

Combined Collection and Analysis of Inorganic and Organic Gunshot Residues

Gunshot residue (GSR) analysis and their interpretation provide crucial information on a criminal investigation involving the use of firearms. To date, several approaches have been proposed for the implementation of a combined sampling and analysis of inorganic (IGSR) and organic GSR (OGSR). However, it is not clear at this stage if concurrent analyses of both types of residue might be detrimental to the analysis of IGSR currently applied in forensic laboratories. Thus, this work aims to compare and evaluate three different protocols for the combined collection and analysis of IGSR and OGSR. These methods, respectively, involve the use of a modified stub (with two halves, one for the detection of IGSR and the other for the analysis of OGSR); the sequential recovery of GSR with two stubs mounted with different adhesives (double-sided carbon tape and Tesa® TACK) and the sequential analysis of IGSR and OGSR from a single carbon stub following carbon deposition. The detection of IGSR was carried out using SEM-EDX, while OGSR analysis was performed using ultra-high-performance liquid chromatography–tandem mass spectrometry (UHPLC-MS/MS). Obtained results for experiments performed using Geco Sinoxid^® ammunition indicated that sequential analysis was the most suitable protocol for the combined collection and analysis of both IGSR and OGSR. A higher number of inorganic (characteristic and consistent) particles and higher concentrations of ethylcentralite, N-nitrosodiphenylamine, diphenylamine, and nitroglycerin were recovered with this method.