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排序方式: 共有109条查询结果,搜索用时 15 毫秒
1.
Ana Celeste Ximenes Oliveira Ph.D. Alexandre Leão Ph.D. Karla Balzuweit Ph.D. Livia Siman Ph.D. Oscar Nassif Mesquita Ph.D. Luiz Orlando Ladeira Ph.D. Luiz Alberto Cury Ph.D. 《Journal of forensic sciences》2019,64(6):1867-1872
The optical and morphological properties of resveratrol were investigated. This nontoxic fluorescent natural material, emitting in the visible blue light, was used as an optical marker, enabling the enhancement of the image contrast coming from relief pictures marked on challenging surfaces. By applying appropriated imaging softwares, this marker was verified to be very useful in the latent fingerprint recognition deposited on different wood surface types, mainly those with high level of roughness, where conventional forensic materials do not allow effective fingerprint image visualization. 相似文献
2.
Marta Concheiro Ana de Castro Oscar Quintela Manuel Lpez-Rivadulla Angelines Cruz 《Forensic Science International Supplement Series》2005,150(2-3):221
This paper describes the analytical methodology for the determination of MDMA, MDA, MDEA and MBDB in oral fluid. After a liquid–liquid extraction, the analysis was carried out by high performance liquid chromatography (HPLC), with fluorescence detection. The detector wavelength was fixed at 285 nm for excitation and 320 nm for emission. The mobile phase, a mixture of phosphate buffer (pH = 5) and acetonitrile (75:25), and the column, Kromasil 100 C8 5 μm 250 mm × 4.6 mm, allowed good separation of the compounds in an isocratic mode in only 10 min. The method was validated and showed good limits of detection (2 ng/mL) and quantitation (10 ng/mL) for all the amphetamine derivatives. No interfering substances were detected. A stability study of these compounds in oral fluid stored at three different temperatures (−18, 4 and 20 °C) over 10 weeks was conducted, showing a time-dependent degradation of the four compounds. 相似文献
3.
Oscar W. Gabriel 《Politische Vierteljahresschrift》2004,45(4):477-478
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Ownership and conditionality in IMF-supported programs: Back to Per Jacobsson’s time 总被引:1,自引:1,他引:0
Oscar Calvo-Gonzalez 《The Review of International Organizations》2007,2(4):329-343
Using a historical case study this article provides an example of how heterogeneity of interests within a government may affect the interplay between country ownership of reforms and conditionality in IMF-supported programs.
The case study also highlights how pro-reformers’ preferences may be conditional on reforms advancing their personal agendas.
This suggests a new issue to be addressed by formal models of conditionality. Two main themes emerge from the analysis: (a)
the importance of a clear hierarchy to unify heterogeneous interests among decision makers; and, (b) a flexible country-tailored
approach to conditionality can contribute to domestic ownership of reforms.
相似文献
Oscar Calvo-GonzalezEmail: |
7.
Andrea Y. Garzón-Serrano M.Sc. César A. Sierra Ph.D. Oscar Rodríguez-Bejarano Dr.Sc. Diana Sinuco Dr.Sc. 《Journal of forensic sciences》2020,65(4):1085-1093
Ammonium nitrate fuel oil is an explosive mixture found in most antipersonnel landmines (APL) buried throughout the Colombian territory. During more than 50 years of internal conflict, the Colombian government has found that trained dogs are the most effective method to detect APL. However, the olfactive signature in ANFO is unknown and also if there are differences in detection related to the explosive manufacturing origin. Therefore, this work begins with the analytical validation of the method used to determine ammonia, in its derivatized form as carbamate, released by home-made ANFO using HS-SPME-GC-FID. Once validated, the method was used to identify ammonia and other organic volatile compounds present in ANFO, under laboratory and simulated field conditions. The validation process includes the evaluation of the optimum conditions for the derivation and extraction of butylcarbamate, the determination of the working ranges with linear response in FID, the limits of detection and quantification, the sensitivity, and the precision. The results of the validation established linearity and sensitivity in a concentration between 20 and 120 mg/L, as well as low limits of detection and quantification of 6.4 and 21.4 mg/L, respectively. Also, an intermediate precision of 11% for butylcarbamate with a repeatability of 8%. The validated method showed in real samples of home-made ANFO besides ammonia, the presence of low molecular methylamines, and also exhibited differences in volatile compositions according to the origin. The objective of this work is to offer a reliable analytical methodology for the extraction and analysis of volatile compounds from ANFO. 相似文献
8.
Oscar W. Gabriel Ulf Bohmann Daniel Gaus Emanuel Richter Annika Frisch Helga Haftendorn Dirk Berg-Schlosser Frank Bönker Dennis-Jonathan Mann Christian Tuschhoff Karsten Schmitz Jared Sonnicksen Heinrich Pehle Marco Schäferhoff Wilhelm Bleek Jürgen Petersen 《Politische Vierteljahresschrift》2009,50(3):646-690
9.
Wolfgang Seibel und Oscar W. Gabriel 《Politische Vierteljahresschrift》2002,43(3):395-396
10.
Schneider PM Bender K Mayr WR Parson W Hoste B Decorte R Cordonnier J Vanek D Morling N Karjalainen M Marie-Paule Carlotti C Sabatier M Hohoff C Schmitter H Pflug W Wenzel R Patzelt D Lessig R Dobrowolski P O'Donnell G Garafano L Dobosz M De Knijff P Mevag B Pawlowski R Gusmão L Conceicao Vide M Alonso Alonso A García Fernández O Sanz Nicolás P Kihlgreen A Bär W Meier V Teyssier A Coquoz R Brandt C Germann U Gill P Hallett J Greenhalgh M 《Forensic science international》2004,139(2-3):123-134
Degradation of human DNA extracted from forensic stains is, in most cases, the result of a natural process due to the exposure of the stain samples to the environment. Experiences with degraded DNA from casework samples show that every sample may exhibit different properties in this respect, and that it is difficult to systematically assess the performance of routinely used typing systems for the analysis of degraded DNA samples. Using a batch of artificially degraded DNA with an average fragment size of approx. 200 bp a collaborative exercise was carried out among 38 forensic laboratories from 17 European countries. The results were assessed according to correct allele detection, peak height and balance as well as the occurrence of artefacts. A number of common problems were identified based on these results such as strong peak imbalance in heterozygous genotypes for the larger short tandem repeat (STR) fragments after increased PCR cycle numbers, artefact signals and allelic drop-out. Based on the observations, strategies are discussed to overcome these problems. The strategies include careful balancing of the amount of template DNA and the PCR cycle numbers, the reaction volume and the amount of Taq polymerase. Furthermore, a careful evaluation of the results of the fragment analysis and of automated allele calling is necessary to identify the correct alleles and avoid artefacts. 相似文献