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通便灵胶囊质量标准的研究
引用本文:李文军 李有军 张卡 马坤芳 都述虎. 通便灵胶囊质量标准的研究[J]. 安徽中医药大学学报, 2007, 0(5): 46-48
作者姓名:李文军 李有军 张卡 马坤芳 都述虎
作者单位:安徽济人药业有限公司,安徽济人药业有限公司,安徽济人药业有限公司,南京医科大学药学院,南京医科大学药学院 安徽亳州236800,安徽亳州236800,安徽亳州236800
摘    要:目的:建立通便灵胶囊的质量标准。方法:以番泻叶、当归为对照药材进行薄层鉴别,采用高效液相色谱法进行含量测定。结果:大黄酸的平均加样回收率为97.16%,RSD=2.23%(n=6)。薄层色谱斑点清晰,阴性对照无干扰,专属性强。结论:该方法结果准确,重复性好,可作为该制剂的质量控制指标。

关 键 词:通便灵胶囊  大黄酸  薄层色谱法  高效液相色谱法
修稿时间:2007-06-04

Study on Quality Standard of Tongbianling Capsules
LI Wen-jun,LI You-jun,ZHANG K,MA Kun-fang,DU Shu-hu. Study on Quality Standard of Tongbianling Capsules[J]. Journal of Anhui Traditional Chinese Medical College, 2007, 0(5): 46-48
Authors:LI Wen-jun  LI You-jun  ZHANG K  MA Kun-fang  DU Shu-hu
Affiliation:Anhui Jiren Pharmaceutical Co. ,Ltd, Anhui Bozhou 230031 ,China
Abstract:Objective:To establish the quality standard of Tongbianling Capsules.Methods:Tongbianling Capsules were identified by thin layer chromatography using Senna Leaf and Chinese Angelica as reference substances.The contents were determined by high performance liquid chromatography.Results:The average recovery of Rhein was 97.16%,and RSD was 2.23%(n=6).Thin layer chromatograph spots were clear.The negative sample had no interference.The Specificity was good.Conclusion:This method is accurate,and it has good repeatability and could be used for the quality control of this preparation.
Keywords:Tongbianling Capsules  Rhein  Thin-layer chromatography  High performance liquid chromatography
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