| 安眠酮及2'-羟甲基安眠酮的毛细柱GC/MS测定 |
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| 引用本文： | 李玉兰,姚希,高利生,徐婉. 安眠酮及2'-羟甲基安眠酮的毛细柱GC/MS测定[J]. 中国法医学杂志, 1988, 0(4) |
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| 作者姓名： | 李玉兰 姚希 高利生 徐婉 |
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| 作者单位： | 公安部第二研究所，公安部第二研究所，公安部第二研究所，公安部第二研究所 |
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| 摘 要： | 作者在 Finnigan Mat 1020 GC/MS 仪上,应用 SE-54熔融硅毛细柱,建立了生物试样中安眠酮、2'-羟甲基安眠酮的分析方法。动物中毒实验表明,此法实用,不仅能检出安眠酮,而且还可检出存在的代谢物;在实际应用中,具有快速、灵敏、准确等特点。检测限为15ng,并已用于刑事案件的鉴定工作中。
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| 关 键 词： | 安眠酮 毛细柱 GC/MS |
DETERMINATION OF METHAQUALONE AND ITS MAJOR METABOLITE,2''''-YDROXYLMETHYLMETHAQUALONE,IN INTERNAL ORGANS BY CAPILLARY COLUMN GC/MS |
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| Li Yulan Yao Xi Gao Lisheng Xu Wan Institute of Forensic Science,Ministry of Public Security,Beijing. DETERMINATION OF METHAQUALONE AND ITS MAJOR METABOLITE,2''''-YDROXYLMETHYLMETHAQUALONE,IN INTERNAL ORGANS BY CAPILLARY COLUMN GC/MS[J]. Chinese Journal of Forensic Medicine, 1988, 0(4) |
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| Authors: | Li Yulan Yao Xi Gao Lisheng Xu Wan Institute of Forensic Science Ministry of Public Security Beijing |
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| Abstract: | An analytical method for the determination of both methaqualone and2'-hydroxymethylmethaqualone in internal organs has been established usingFinnigan Mat 1020 GC/MS instrument with SE-54 fused-silica capillary co-lumn.The animal experiment shows that this method is applicable.Notonly the methaqualone but also its metabolite can be detected using thismethod.This method is rapid,sensitive and accurate.The detection limitis 15μg/ml.The method has been successfully used in criminal cases. |
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| Keywords: | Methaqualone Capillary column GC/MS |
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