| 静松灵的检验 |
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| 引用本文： | 梁恺军,李长立. 静松灵的检验[J]. 刑事技术, 2000, 0(1): 17-18 |
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| 作者姓名： | 梁恺军 李长立 |
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| 作者单位： | 山东省济南市公安局刑警支队 250002(梁恺军，李长立)，山东省济南市公安局刑警支队 250002(张继红) |
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| 摘 要： | 本实验建立了用固相萃取(SPE)、薄层色谱和气—质联用法(GC-MS)分析血、尿、肝中静松灵的方法,在1g尿、血、肝中添加0.01mg药物、回收率分别为96.1%、90%、67%.该方法简单快速准确,经动物实验及案件鉴定验证,效果较好.
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| 关 键 词： | 固相萃取 TLC GC-MS 静松灵 |
DETECTION OF XYLAZOLI IN URINE, BLOOD AND LIVER SPECIMENS |
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| Zhang Kaijun,Li Changli,Zhang Jihong Criminal police detachment of Ji Nan city. DETECTION OF XYLAZOLI IN URINE, BLOOD AND LIVER SPECIMENS[J]. Forensic Science and Technology, 2000, 0(1): 17-18 |
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| Authors: | Zhang Kaijun Li Changli Zhang Jihong Criminal police detachment of Ji Nan city |
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| Affiliation: | Zhang Kaijun,Li Changli,Zhang Jihong Criminal police detachment of Ji Nan city,250002 |
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| Abstract: | : In this paper we reported a method for determining the Xylazoli in urine, blood and liver using solid phase extraction(SPE), thin -layer chromatography(TLC) and gas chromatography/mass spectrometry(GC/MS) . For urine, blood and liver specimens recoveries are 96. 1%, 90. 0% and 67. 0% respectively. We have used this method in some cases sucessfully. |
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| Keywords: | xylazoli urine blood liver solid phase extraction |
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