| 用气相色谱法/电子捕获检测器测定尿液中的三唑仑 |
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| 引用本文： | Liu W. 用气相色谱法/电子捕获检测器测定尿液中的三唑仑[J]. 法医学杂志, 1998, 14(4): 203, 208, 251 |
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| 作者姓名： | Liu W |
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| 作者单位： | 司法部司法鉴定科学技术研究所!上海,200063 |
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| 摘 要： | 建立了用气相色谱／电子捕获检测器测定尿液中三唑仑含量的方法。2ml尿样在破性条件下用2ml×2氯仿提取净化后,60℃水浴下用空气吹干,残留物用环己烷定容溶解后,进气相色谱仪分析,三唑仑的保留时间为10．74min。最低检测限为0．5ng／ml,回收率为95．98％,变异系数为7．85％（n＝5）。在2～50ng／ml浓度范围内有良好的线性关系：A＝－67．9＋570．IC,r＝0．9939。
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| 关 键 词： | 三唑仑 气相色谱法吨子捕获检测器 尿液 |
Determination of triazolam in human urine by GC/ECD |
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| Liu W. Determination of triazolam in human urine by GC/ECD[J]. Journal of Forensic Medicine, 1998, 14(4): 203, 208, 251 |
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| Authors: | Liu W |
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| Affiliation: | Institute of Forensic Sciences, Ministry of Justice, PR. China, Shanghai 200063. |
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| Abstract: | A GC/ECD method was established to determine triazolam in human urine qualitatively and quantitatively. The triazolam was extracted from 2ml urine with 2 x 2ml chloroform.The retention time of triazolam was 10. 74 min. The limit ofthe determination was 0. 5ng/ml. The recovery of the procedure in 5 ng/ml was 95.98%, CV = 7. 85% (n = 5). Thelimit of quantitation is 2 - 50ng/ml. |
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| Keywords: | triazolam GC/ECD urine |
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