| 合成大麻素类新精神活性物质4F-MDMB-BICA的检测 |
| |
| 引用本文： | 王跨陡,袁晓亮,张玉荣,盛振海,胡钧健,曹芳琦. 合成大麻素类新精神活性物质4F-MDMB-BICA的检测[J]. 中国法医学杂志, 2021, 0(1): 25-29 |
| |
| 作者姓名： | 王跨陡 袁晓亮 张玉荣 盛振海 胡钧健 曹芳琦 |
| |
| 作者单位： | 1.上海市公安局物证鉴定中心上海市现场物证重点实验室;2.上海市刑事科学技术研究院上海市现场物证重点实验室 |
| |
| 基金项目： | 国家自然科学基金青年科学基金项目(81701864);上海市优秀学术带头人计划资助(19XD1432700);上海市青年科技启明星计划资助(18QB1403400);上海市自然科学基金探索类项目(17ZR1441600)。 |
| |
| 摘 要： | 目的 建立基于红外光谱(fourier transform infrared,FT-IR)、气相色谱-质谱联用(gas chromatography-mass spectrometry,GC-MS)、高分辩质谱(high resolution mass spectrometer,HRMS)和核磁共振波谱(nuclear...
|
| 关 键 词： | 合成大麻素 4F-MDMB-BICA 气相色谱-质谱 高分辨质谱 核磁共振波谱 |
Detection of 4F-MDMB-BICA,a new synthetic cannabinoid psychoactive substance |
| |
| Wang Kuadou,Yuan Xiaoliang,Zhang Yurong,Sheng Zhenhai,Hu Junjian,Cao Fangqi. Detection of 4F-MDMB-BICA,a new synthetic cannabinoid psychoactive substance[J]. Chinese Journal of Forensic Medicine, 2021, 0(1): 25-29 |
| |
| Authors: | Wang Kuadou Yuan Xiaoliang Zhang Yurong Sheng Zhenhai Hu Junjian Cao Fangqi |
| |
| Affiliation: | (Institute of Forensic Science of Shanghai Public Security Bureau,Shanghai 200083,China;Shanghai Research Institute of Criminal Science and Technology,Shanghai 200083,China) |
| |
| Abstract: | Objective To establish a method based on FT-IR,GC-MS,HRMS and NMR,so as to identify new psychoactive substance of Synthetic cannabinoids.Method The samples were detected by FT-IR,GC-MS,HRMS(solvent is methanol)and NMR(solvent is deuterated methanol).Results The characteristic ions(m/z)of the main components in the sample was 218(base peak),362、306、274、246、144、116 respectively by GC-MS.The accurate mass of protonated molecular ion([M+H]+)measureed by HRMS was 363.20774.The data analysis of FT-IR,GC-MS and HRMS showed that the unknown sample was a new synthetic cannabinoid psychoactive substance,4F-MDMBBICA.Conclusion The established method can be used to identify 4 F-MDMB-BICA in unknown samples.The method is fast,convenient,reliable and practical,which can provide reference for the detection and identification of cases involving such substances in the future. |
| |
| Keywords: | Synthetic cannabinoids 4F-MDMB-BICA GC-MS HRMS NMR |
| 本文献已被 CNKI 维普 等数据库收录！ |
|
