| GC/MS法联合分析生物检材中的尼美舒利、二氧丙嗪 |
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| 引用本文： | 张兆宏,刘春芳,李国庆.GC/MS法联合分析生物检材中的尼美舒利、二氧丙嗪[J].刑事技术,2012(5):22-24. |
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| 作者姓名： | 张兆宏 刘春芳 李国庆 |
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| 作者单位： | 1. 山东省潍坊市公安局,261061
2. 山东省安丘市公安局,262100 |
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| 摘 要： | 目的建立生物检材中尼美舒利、二氧丙嗪的GC/MS检验方法。方法采用浸取法提取,GC/MS定性检验,内标法选择离子检测（SIM）模式定量检验。结果最低回收率为69%,尼美舒利的线性相关系数为0.998,克咳敏的线性相关系数为0.9973。结论该方法操作简便快速,提取率高,可用于实际案件中尼美舒利、二氧丙嗪的检验。
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| 关 键 词： | 尼美舒利 二氧丙嗪 液固浸提 气相色谱-质谱联用仪 |
Analysis of nimesulide and dioxopromethazine in biological sample by GC/MS |
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| ZHANG Zhao-hong
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LIU Chun-fang
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LI Guo-qing.Analysis of nimesulide and dioxopromethazine in biological sample by GC/MS[J].Forensic Science and Technology,2012(5):22-24. |
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| Authors: | ZHANG Zhao-hong LIU Chun-fang LI Guo-qing |
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| Institution: | (Wei fang Pwblic Security Bureau, Shandong 261061 , China) |
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| Abstract: | Objective To develop a GC/MS method for determination of nimesulide and dioxopromethazine from biological sample. Methods The nimesulide and dioxopromethazine were extracted by immersion method, qualitative analyzed by GC/MS and quantitative analyzed by GC/MS with selected ion monitoring mode （SIM）. Results The lowest recovery rate was 69%, the linear correlation coefficient of nimesulide was 0. 998, the linear correlation coefficient of dioxopromethazine was 0. 9973. Conclusion The method is easy and reliable. |
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| Keywords: | nimesulide dioxopromethazine immersion GC/MS |
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