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Analysis of alkyl nitrites by capillary gas chromatography-mass spectrometry |
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| Authors: | T S Bal D R Gutteridge A A Hiscutt B Johnson I Oxley |
| Affiliation: | 1. London Metropolitan University, 166-220 Holloway Road, N7 8DB London, UK;2. Nu Instruments Ltd., Unit 74, Clywedog Road South, Wrexham LL13 9XS, UK;3. IFW Dresden, Helmholtzstraße 20, 01069 Dresden, Germany;4. Blackett Laboratory, Imperial College, London SW7 2BZ, UK;5. Evans Analytical Group, 103 Commerce Blvd, Liverpool, NY 13088, USA;1. Centre d''Etudes Supérieures de la Rennaissance, Université François Rabelais, Tours, France;2. Centre de Référence Maladies Neuromusculaires Nantes-Angers, CHU de Nantes, Nantes, France;3. Atlantic Gene Therapy Institute, Nantes, France |
| Abstract: | This paper presents the analysis of the commonly-abused alkyl nitrites by capillary column gas chromatography-mass spectrometry. It includes the procedure for the preparation of the relevant alkyl nitrites which can be used as a source of reference compounds. The retention index data and the eight most intense peaks in the mass spectra of iso-butyl, iso-pentyl(amyl) and some closely-related nitrites are given. |
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