| 顶空色谱法测定解剖组织中的丁酮 |
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| 引用本文： | 刘久华. 顶空色谱法测定解剖组织中的丁酮[J]. 中国法医学杂志, 1990, 0(4) |
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| 作者姓名： | 刘久华 |
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| 作者单位： | 河北省公安厅 石家庄 |
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| 摘 要： | 本文研究了人体组织中丁酮的顶空色谱测定方法。该方法以丙酮为内标,测得丁酮在肝、肾、血样品中的添加回收率大于75%。最小检出量为1ppm。经对一丁酮中毒死者解剖组织测定,丁酮的含量为肝0. 06mg/g,肾0. 23mg/g,血0. 47mg/ml。
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| 关 键 词： | 丁酮 丙酮 顶空色谱法 |
DETERMINATION OF BUTANONE LEVELS IN POSTMORTEM HUMAN TISSUES SAMPLES BY HEADSPACE GAS CHROMATOGRAPHY |
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| Liu Jiuhua Public Secvrity Bureau of Hebei Province,Shijiazhuang. DETERMINATION OF BUTANONE LEVELS IN POSTMORTEM HUMAN TISSUES SAMPLES BY HEADSPACE GAS CHROMATOGRAPHY[J]. Chinese Journal of Forensic Medicine, 1990, 0(4) |
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| Authors: | Liu Jiuhua Public Secvrity Bureau of Hebei Province Shijiazhuang |
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| Abstract: | A headspace gas choromatographic method has been developed for the deter-mination of butanone level in postmortem human samples,this method usedacetome as intermal standard.The added recovery rates from liver,kidney andblood samples were higher than 75%.The minimun detectable amount was 1ppm.The butanone levels in postmortem human tissue samples from one poisoned casewere as follows.0. 06 mg/g in Liver,0. 23 mg/g in kidney,and 0. 47 mg/ml in blood. |
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| Keywords: | Butanone Acetone Headspace gas chromatography |
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