| 用五氟苄基溴对五氯酚进行衍生化的方法 |
| |
| 引用本文： | 傅得锋,徐豫青. 用五氟苄基溴对五氯酚进行衍生化的方法[J]. 刑事技术, 2002, 0(6): 15-16 |
| |
| 作者姓名： | 傅得锋 徐豫青 |
| |
| 作者单位： | 浙江省公安厅刑事侦查总队,杭州,310009 |
| |
| 摘 要： | 目的五氟苄基溴(PFBBr)衍生化试剂对五氯酚进行衍生化研究。方法运用GC/MS、GC/ECD印证分析衍生化产物。结果改变了五氯酚的挥发性,提高检测灵敏度,在本文控制的实验条件下,五氯酚-PFBBr衍生物的检测限可达1pg。结论为检测微量五氯酚提供了一种有效手段。
|
| 关 键 词： | GC/MS 五氯酚 五氟苄基溴 GC/ECD |
| 文章编号： | 1008-3650(2002)06-015-02 |
| 修稿时间： | 2001-12-12 |
Study on the derivative of pentachorophenol produced by using the reagent pfbbr |
| |
| Fu Defeng,Xu Yuqing. Study on the derivative of pentachorophenol produced by using the reagent pfbbr[J]. Forensic Science and Technology, 2002, 0(6): 15-16 |
| |
| Authors: | Fu Defeng Xu Yuqing |
| |
| Abstract: | The devivative of pentachlorophenol(PCP)produced by the deriation re ag ent PFBBr is analyzed by GC/MS and GC/ECD.The volatility of PCP is suppres sed and the sensitivity of detection is raised by derivation.The proposed metho d can be used effectively for the determination of microamounts of PCP. |
| |
| Keywords: | GC/MS PCP PFBBr GC/ECD. |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
