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Implementation and Optimization of the Sodium‐Rhodizonate Method for Chemographic Shooting Distance Estimation
Authors:Nadia Geusens B.Sc.  Bart Nys Ph.D.  Sébastien Charles Ph.D.
Affiliation:1. National Institute for Criminalistics and Criminology‐Criminalistics, Vilvoordsesteenweg, 100 1120 Neder‐over‐heembeek, Brussels, Belgium Corresponding author: Nadia Geusens, B.Sc. E‐mail:;2. National Institute for Criminalistics and Criminology‐Criminalistics, Vilvoordsesteenweg, 100 1120 Neder‐over‐heembeek, Brussels, Belgium
Abstract:In shooting incident investigations where it is important to estimate the shooting distance, the sodium‐rhodizonate coloring method has been used for the visualization of GSR patterns extensively. This publication describes the optimization of this method by the use of a heated press for the transfer of GSR traces on garments, as well as variation of a number of other important process parameters. Our final aim for this project was to prepare a formal validation of the coloring method as prerequisite for its inclusion into the scope of ISO17025‐certified methods in the GSR Laboratory. A number of important factors and process parameters were identified, such as buffer composition and pH, type of textile used as a substrate and resolution of the documentation of the results. Results were tested using a synthetic proficiency test. Our optimized method has been found to be a very effective technique for visualization of macroscopic GSR traces.
Keywords:forensic science  gunshot residue analysis  shooting distance determination  sodium‐rhodizonate test  gunshot residue pattern visualization  optimization of laboratory method  implementation of a hot press
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