| N-甲基-3,4-亚甲二氧基卡西酮的确证 |
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| 引用本文： | 黄星,王蔚昕,徐鹏,赵阳,张春水,朱军,高利生. N-甲基-3,4-亚甲二氧基卡西酮的确证[J]. 中国法医学杂志, 2012, 27(6): 474-476 |
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| 作者姓名： | 黄星 王蔚昕 徐鹏 赵阳 张春水 朱军 高利生 |
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| 作者单位： | 公安部物证鉴定中心,北京,100038 |
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| 基金项目： | 公安部应用创新计划资助项目(2012YYCXGAES115);公安部物证鉴定中心基本科研业务费专项资金资助项目(2012JBYY009) |
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| 摘 要： | 目的 对毒品案件样本进行N-甲基-3,4-亚甲二氧基卡西酮(bk-MDMA)确证检验.方法 采用阴离子检测、颜色反应、气质联用(GC/MS)、核磁共振(NMR)、傅立叶变换红外光谱(FTIR)等方法对毒品案件中白色晶体样本进行剖析确证.结果 快速筛查结果提示样本为具有亚甲二氧基结构的仲胺物质的盐酸盐,经GC/MS、NMR、FTIR检验,确证样本为bk-MDMA,系3,4-亚甲二氧基甲基苯丙胺(3,4-methylenedioxymethamphetmaine,MDMA)的卡西酮类似物.结论 采用本文所用方法可以对毒品案件样本中N-甲基-3,4-亚甲二氧基卡西酮成分进行确证,该药具有滥用的可能性应引起相关部门的重视.
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| 关 键 词： | 法医毒物分析 N-甲基-3,4-亚甲二氧基卡西酮 核磁共振 气质联用 傅立叶红外变换 |
Identification of N-methyl-3,4-methylenedioxycathinone from the unknown white crystalline substance |
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| Huang Xing,Wang Weixin,Xu Peng,Zhao Yang,Zhang Chunshui,Zhu Jun,Gao Lisheng. Identification of N-methyl-3,4-methylenedioxycathinone from the unknown white crystalline substance[J]. Chinese Journal of Forensic Medicine, 2012, 27(6): 474-476 |
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| Authors: | Huang Xing Wang Weixin Xu Peng Zhao Yang Zhang Chunshui Zhu Jun Gao Lisheng |
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| Affiliation: | / Institute of Forensic Science,Ministry of Public Security,Beijing 100038,China) |
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| Abstract: | Objective To identify the white crystalline substance concealed in an envelope which was delivered by police to our laboratory.Methods The white crystalline substance was screened by anion test and colour tests,then the presence of bk-MDMA was confirmed by GC/MS and NMR.FTIR was also used for characterization of bk-MDMA.Results N-methyl-3,4-methylenedioxycathinone(aka methylone,bk-MDMA) was detected recently by the drug laboratory of IFS(Institute of Forensic Science).Conclusion This is the first report of finding N-methyl-3,4-methylenedioxycathinone in China Mainland.It is suggested that more attention should be paid on cathinone family designer drugs in Asia. |
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| Keywords: | forensic toxicology analysis N-methyl-3,4-methylenedioxycathinone NMR GC/MS FTIR |
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