| ASE和GPC方法检验非苯二氮卓类催眠药 |
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| 引用本文： | 张蕾萍,舒翠霞,杜鸿雁. ASE和GPC方法检验非苯二氮卓类催眠药[J]. 刑事技术, 2012, 0(3): 6-8 |
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| 作者姓名： | 张蕾萍 舒翠霞 杜鸿雁 |
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| 作者单位： | 1. 公安部物证鉴定中心,北京,100038
2. 中国医科大学,辽宁沈阳,110001 |
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| 摘 要： | 目的建立生物样品中4种非苯二氮卓类新型催眠药的快速溶剂萃取-凝胶色谱检验方法。方法生物样品采用快速溶剂萃取，凝胶色谱净化，GC／NPD检验。结果4种新型催眠药的平均回收率均在83％以上，检测限为0．05μg·mL-1～0．1μg·mL-1。结论该方法可满足实际检案的需求。
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| 关 键 词： | 非苯二氮卓类催眠药 快速溶剂萃取 凝胶色谱 气相色谱法 |
Analysis of nonbenzodiazepine hypnotic in biology samples by ASE and GPC-GC |
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| ZHANG Lei-ping , SHU Cui-xia , DU Hong-yan. Analysis of nonbenzodiazepine hypnotic in biology samples by ASE and GPC-GC[J]. Forensic Science and Technology, 2012, 0(3): 6-8 |
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| Authors: | ZHANG Lei-ping SHU Cui-xia DU Hong-yan |
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| Affiliation: | (Institute of Forensic Science,Ministry of Public Security,Beijing 100038,China) |
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| Abstract: | Objective To develop ASE-GPC method for analysis of nonbenzodiazepine hypnotic in biology samples.Methods The nonbenzodiazepine hypnotic was extracted with accelerated solvent extraction,cleaned by auto gel permeation chromatography and then the collected solution was analyzed by GC/NPD.Results The recovery rate is 83%,the limits of detection is 0.05～0.1μg·mL-1.Conclusion ASE and GPC method can be used in forensic toxicological analysis. |
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| Keywords: | nonbenzodiazepine hypnotic accelerated solvent extraction gel permeation chromatography GC |
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