| GC／ECD、GC／MS法检验焚烧尸体组织中安定和舒乐安定 |
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| 引用本文： | 王炯,赵敬真,刘健,侯占伟. GC／ECD、GC／MS法检验焚烧尸体组织中安定和舒乐安定[J]. 刑事技术, 2003, 0(5): 22-23 |
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| 作者姓名： | 王炯 赵敬真 刘健 侯占伟 |
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| 作者单位： | 1. 公安部物证鉴定中心,北京,100038
2. 公安大学研究生进修班,北京,100038 |
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| 摘 要： | 目的建立GC/ECD、GC/MS分析焚烧尸体肝组织中安定、舒乐安定的方法。方法采用酸性丙酮-水浸提、液-液分配净化的方法,以HP6890GC/ECD、OV-1701石英毛细管柱和岛津QP5050ADB-5MS石英毛细柱分析方法。结果该提取方法的回收率安定81.2%、舒乐安定75.8%,焚烧尸体肝组织中的含量:安定0.060μg/g,舒乐安定0.330μg/g。结论该方法操作简单,准确可靠,适用于中毒案件鉴定。
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| 关 键 词： | 焚烧尸体 肝 安定 舒乐安定 |
| 文章编号： | 1008-3650(2003)05-0022-02 |
| 修稿时间： | 2003-01-06 |
Detection of diazepam and estazolam in burned corpse tissue by GC/ECD & GC/MS |
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| WANG Jiong ,ZHAO Jing-zhen,LIU Gian,et al. Detection of diazepam and estazolam in burned corpse tissue by GC/ECD & GC/MS[J]. Forensic Science and Technology, 2003, 0(5): 22-23 |
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| Authors: | WANG Jiong ZHAO Jing-zhen LIU Gian et al |
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| Affiliation: | WANG Jiong 1,ZHAO Jing-zhen,LIU Gian,et al |
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| Abstract: | The samples of the liver tissue of a burned corpse from a poison case were extracted by acidic aceton-water and analysed by GC/ECD and GC/MS.Diazepam and estazolam were found in the burned corpse.Also the contents of the two medicne were determined. |
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| Keywords: | burned corpse corpseliver diazepam estazolam acidic acetone-water |
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