| 东莨菪碱的GC／MS检验 |
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| 引用本文： | Chu JX,Xie Y,Zhuo XC. 东莨菪碱的GC／MS检验[J]. 法医学杂志, 2006, 22(4): 285-287 |
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| 作者姓名： | Chu JX Xie Y Zhuo XC |
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| 作者单位： | 1. 浙江省人民检察院,浙江,杭州,310012
2. 杭州市萧山区公安分局,浙江,杭州,311200 |
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| 摘 要： | 目的用气质联用方法分离定性案件检材中微量的东莨菪碱成分。方法以液-液萃取法提取分离,用CP5860(CP-sil8CB)毛细管拄(30m×0.25mm×0.33!m),并采用气质联用仪(GC/MS)测定东莨菪碱。结果可检出检材中微量东莨菪碱,色谱分离良好。结论以气质联用仪(GC/MS)测定东莨菪碱方法灵敏度高,测定结果准确可靠。
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| 关 键 词： | 东莨菪碱 中毒 GC/MS |
| 文章编号： | 1004-5619(2006)04-0285-03 |
| 修稿时间： | 2006-04-18 |
Determination of scopolamine in the poisoning case by GC/MS |
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| Chu Jian-Xin,Xie Yu,Zhuo Xiao-Cong. Determination of scopolamine in the poisoning case by GC/MS[J]. Journal of Forensic Medicine, 2006, 22(4): 285-287 |
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| Authors: | Chu Jian-Xin Xie Yu Zhuo Xiao-Cong |
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| Affiliation: | The Procuratorate of Zhejiang Province, Hangzhou 310012, China. |
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| Abstract: | OBJECTIVE: To separate and determine scopolamine from the food in a poisoning case by GC/MS. METHODS: The scopolamine was determined by GC/MS/El used CP5860(CP-sil8CB) column (30 mx 0.25 mmx 0.33 microm) with liquid- liquid extraction. RESULTS: The deny scopolamine was found in the case sample, and the chromatographic separation of the peaks is fine. CONCLUSION: The method is accurate and reliable. |
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| Keywords: | scopolamine Poisoning GC/MS |
| 本文献已被 CNKI 维普 万方数据 PubMed 等数据库收录！ |
