| GC/MS/Xcalibur技术自动分析疑似固体中管制药物 |
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| 引用本文： | 黎乾,邢若葵,戴维列,温锦锋,王松才,黄炜. GC/MS/Xcalibur技术自动分析疑似固体中管制药物[J]. 中国司法鉴定, 2013, 0(1): 42-45 |
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| 作者姓名： | 黎乾 邢若葵 戴维列 温锦锋 王松才 黄炜 |
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| 作者单位： | 广州市刑事科学技术研究所,广东广州,510030 |
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| 基金项目： | 公安部应用创新项目(2009YYCXGD51068) |
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| 摘 要： | 目的建立疑似含毒检材中国家管制药品的自动筛选方法。方法以我国2007年公布的精神药品和麻醉药品的品种目录为检测目标物,建立质谱用户库;以此为基础,设置气质联用仪自动分析方法对疑拟检材进行常见管制药品的快速筛选。结果建立了库名含多种实用信息、包括230种管制药品的质谱用户库;建立管制药品的质谱自动分析方法,实现＂一针分析出结果＂。结论方法简单、快速、准确可靠,省时省力,能有效提高可疑检材中管制药品筛选分析的速度。
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| 关 键 词： | 管制药物 精神药品及麻醉药品 质谱自动分析方法 快速筛选 |
Automatic Detection of Control Drugs with GC/MS-Xcalibur |
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| LI Qian,XING Ruo-Kui,DAI Wei-lie,WEN Jin-Feng,WANG Song-cai,HUANG Wei. Automatic Detection of Control Drugs with GC/MS-Xcalibur[J]. Chinese Journal of Forensic Sciences, 2013, 0(1): 42-45 |
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| Authors: | LI Qian XING Ruo-Kui DAI Wei-lie WEN Jin-Feng WANG Song-cai HUANG Wei |
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| Affiliation: | (Institute of Forensic Science,Guangzhou Municipal Public Security Bureau,Guangzhou 510030,China) |
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| Abstract: | Objective To develop an automatic screening method for the identification of national control drugs.Method A mass spectrum library of national control drugs on the list of Narcotic Drugs and Psychotropic Substances under National Control（2007） was established.Then,with an automatic GC/MS method,common control drugs in suspected samples were screened rapidly.Results A library containing the mass spectra of 230 national control drugs and related useful information has been built.An automated screening method for control drugs with GC/MS has been set up.Conclusion The method is simple,quick and reliable.It can be used for the rapid screening of national control drugs in suspected samples. |
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| Keywords: | national control drug psychotropic substance and narcotic drug automatic mass spectrum analysis method rapid screening |
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